Technology Process of C28H39N3O8
There total 4 articles about C28H39N3O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
tetrahydrofuran;
at 20 ℃;
for 0.2h;
Molecular sieve;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium cyanoborohydride / dichloromethane; methanol / 1.5 h / Molecular sieve
2: dicyclohexyl-carbodiimide; 2,4,6-trimethyl-pyridine; ethyl cyanoglyoxylate-2-oxime / dichloromethane / 3 h / 20 °C
3: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0.2 h / 20 °C / Molecular sieve
With
2,4,6-trimethyl-pyridine; sodium cyanoborohydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; ethyl cyanoglyoxylate-2-oxime;
In
tetrahydrofuran; methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dicyclohexyl-carbodiimide; 2,4,6-trimethyl-pyridine; ethyl cyanoglyoxylate-2-oxime / dichloromethane / 3 h / 20 °C
2: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0.2 h / 20 °C / Molecular sieve
With
2,4,6-trimethyl-pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; ethyl cyanoglyoxylate-2-oxime;
In
tetrahydrofuran; dichloromethane;