2-methyl-2-propanyl (3-chloro-2-oxopropyl)phenylcarbamate

Base Information

Chemical Name:2-methyl-2-propanyl (3-chloro-2-oxopropyl)phenylcarbamate
CAS No.:1260085-90-2
Molecular Formula:C₁₄H₁₈ClNO₃
Molecular Weight:283.755
Hs Code.:

Synonyms:2-methyl-2-propanyl (3-chloro-2-oxopropyl)phenylcarbamate

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Chemical Property of 2-methyl-2-propanyl (3-chloro-2-oxopropyl)phenylcarbamate

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Technology Process of 2-methyl-2-propanyl (3-chloro-2-oxopropyl)phenylcarbamate

There total 4 articles about 2-methyl-2-propanyl (3-chloro-2-oxopropyl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1260086-06-3
tert-butyl 3-chloro-2-hydroxypropyl(phenyl)carbamate

: 1260085-90-2
2-methyl-2-propanyl (3-chloro-2-oxopropyl)phenylcarbamate

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 0.5h; regioselective reaction;
DOI:10.1055/s-0030-1257938

Reference yield: 78.0%

: 593-71-5
Chloroiodomethane

: 1444623-79-3
2-methyl-2-propanyl {2-[methoxy(methyl)amino]-2-oxoethyl}phenylcarbamate

: 1260085-90-2
2-methyl-2-propanyl (3-chloro-2-oxopropyl)phenylcarbamate

Guidance literature:: With methyllithium lithium bromide; In tetrahydrofuran; diethyl ether; nitrogen; at -90 ℃; for 1h; liquid N₂;
DOI:10.1002/adsc.201201043

Reference yield:

: 1250901-32-6
N-methoxy-N-methyl-N²-phenylglycinamide

: 1260085-90-2
2-methyl-2-propanyl (3-chloro-2-oxopropyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / ethanol / Reflux

2: methyllithium lithium bromide / tetrahydrofuran; nitrogen; diethyl ether / 1 h / -90 °C / liquid N₂

With methyllithium lithium bromide; sodium carbonate; In tetrahydrofuran; diethyl ether; ethanol; nitrogen;
DOI:10.1002/adsc.201201043