10-(3,5-dimethoxybenzyl)-9,10-dihydro-10-(3-methoxybenzyl)-9-anthracenol

Base Information

Chemical Name:10-(3,5-dimethoxybenzyl)-9,10-dihydro-10-(3-methoxybenzyl)-9-anthracenol
CAS No.:887617-52-9
Molecular Formula:C₃₁H₃₀O₄
Molecular Weight:466.577
Hs Code.:

Synonyms:10-(3,5-dimethoxybenzyl)-9,10-dihydro-10-(3-methoxybenzyl)-9-anthracenol

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Chemical Property of 10-(3,5-dimethoxybenzyl)-9,10-dihydro-10-(3-methoxybenzyl)-9-anthracenol

Chemical Property:

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Technology Process of 10-(3,5-dimethoxybenzyl)-9,10-dihydro-10-(3-methoxybenzyl)-9-anthracenol

There total 3 articles about 10-(3,5-dimethoxybenzyl)-9,10-dihydro-10-(3-methoxybenzyl)-9-anthracenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 564468-49-1
10-(3,5-dimethoxy-benzylidene)-10H-anthracen-9-one

: 887617-52-9
10-(3,5-dimethoxybenzyl)-9,10-dihydro-10-(3-methoxybenzyl)-9-anthracenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 85 percent / H₂ / Pd/C / ethyl acetate; methanol / 20 °C

2.1: 77 percent / potassium hydroxide; 18-crown-6; potassium iodide / acetone / 60 °C

3.1: NaBH₄ / bis-(2-methoxy-ethyl) ether / 0.5 h

3.2: NaBH₄; methanol / bis-(2-methoxy-ethyl) ether / 4 h

With potassium hydroxide; sodium tetrahydroborate; 18-crown-6 ether; hydrogen; potassium iodide; palladium on activated charcoal; In methanol; diethylene glycol dimethyl ether; ethyl acetate; acetone;
DOI:10.1021/jo0526791

Reference yield:

: 887617-47-2
10-(3,5-dimethoxybenzyl)-10-(3-methoxybenzyl)-9(10H)-anthracenone

: 887617-52-9
10-(3,5-dimethoxybenzyl)-9,10-dihydro-10-(3-methoxybenzyl)-9-anthracenol

Guidance literature:: 10-(3,5-dimethoxybenzyl)-10-(3-methoxybenzyl)-9(10H)-anthracenone; With sodium tetrahydroborate; In diethylene glycol dimethyl ether; for 0.5h;

With methanol; sodium tetrahydroborate; In diethylene glycol dimethyl ether; for 4h;
DOI:10.1021/jo0526791

Reference yield:

: 579504-84-0
10-(3,5-dimethoxybenzyl)-9(10H)-anthracenone

: 887617-52-9
10-(3,5-dimethoxybenzyl)-9,10-dihydro-10-(3-methoxybenzyl)-9-anthracenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 77 percent / potassium hydroxide; 18-crown-6; potassium iodide / acetone / 60 °C

2.1: NaBH₄ / bis-(2-methoxy-ethyl) ether / 0.5 h

2.2: NaBH₄; methanol / bis-(2-methoxy-ethyl) ether / 4 h

With potassium hydroxide; sodium tetrahydroborate; 18-crown-6 ether; potassium iodide; In diethylene glycol dimethyl ether; acetone;
DOI:10.1021/jo0526791