C₂₈H₅₀O₅Si₂

Base Information

Chemical Name:C₂₈H₅₀O₅Si₂
CAS No.:1254331-96-8
Molecular Formula:C₂₈H₅₀O₅Si₂
Molecular Weight:522.873
Hs Code.:

C<sub>28</sub>H<sub>50</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₂₈H₅₀O₅Si₂

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Chemical Property of C₂₈H₅₀O₅Si₂

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Technology Process of C₂₈H₅₀O₅Si₂

There total 6 articles about C₂₈H₅₀O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1254331-84-4
(E,2S,6S)-8-(4-methoxybenzyloxy)-2,6-di(tert-butyldimethylsilyloxy)oct-4-enenitrile

: 1254331-96-8
C₂₈H₅₀O₅Si₂

Guidance literature:: With diisobutylaluminium hydride; In n-heptane; toluene; at -78 - -10 ℃; for 9h;
DOI:10.1021/ol1021417

Reference yield:

: 1254331-93-5
(S)-4-(4-methoxybenzyloxy)-2-hydroxybutanenitrile

: 1254331-96-8
C₂₈H₅₀O₅Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1H-imidazole / dichloromethane / 24 h / 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / toluene; n-heptane / 9 h / -78 - -10 °C / Inert atmosphere

3.1: tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere

3.2: 3 h / -78 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / toluene; n-heptane / 9 h / -78 - -10 °C / Inert atmosphere

With 1H-imidazole; diisobutylaluminium hydride; In tetrahydrofuran; n-heptane; dichloromethane; toluene; 3.1: |Julia-Kocienski Olefination / 3.2: |Julia-Kocienski Olefination;
DOI:10.1021/acs.joc.8b02034

Reference yield:

: 1254331-94-6
(S)-4-(4-methoxybenzyloxy)-2-(tert-butyldimethylsilyloxy)butanenitrile

: 1254331-96-8
C₂₈H₅₀O₅Si₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / toluene; n-heptane / 9 h / -78 - -10 °C / Inert atmosphere

2.1: tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere

2.2: 3 h / -78 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / toluene; n-heptane / 9 h / -78 - -10 °C / Inert atmosphere

With diisobutylaluminium hydride; In tetrahydrofuran; n-heptane; toluene; 2.1: |Julia-Kocienski Olefination / 2.2: |Julia-Kocienski Olefination;
DOI:10.1021/acs.joc.8b02034