1,3-bis(2-tert-butylphenyl)imidazolium chloride

Base Information

Chemical Name:1,3-bis(2-tert-butylphenyl)imidazolium chloride
CAS No.:1093348-03-8
Molecular Formula:C₂₃H₂₉N₂*Cl
Molecular Weight:368.95
Hs Code.:

Synonyms:1,3-bis(2-tert-butylphenyl)imidazolium chloride

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Chemical Property of 1,3-bis(2-tert-butylphenyl)imidazolium chloride

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Technology Process of 1,3-bis(2-tert-butylphenyl)imidazolium chloride

There total 1 articles about 1,3-bis(2-tert-butylphenyl)imidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 552841-75-5
N,N'-bis(2-tert-butylphenyl)ethane-1,2-diimine

: 3188-13-4
ethyl chloromethyl ether

: 1093348-03-8
1,3-bis(2-tert-butylphenyl)imidazolium chloride

Guidance literature:: In tetrahydrofuran; water; at 40 ℃; for 18h;

Reference yield: 96.0%

: 103-83-3
N,N'-dimethylbenzylamine

: 1093348-03-8
1,3-bis(2-tert-butylphenyl)imidazolium chloride

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: palladium dichloride

: (1,3-bis(2-tert-butylphenyl)imidazolyl-2-ylidene)Pd(N,N-dimethylbenzylamine(-1H)-κ2N,C)I

Guidance literature:: With K₂CO₃; In acetonitrile; High Pressure; MeCN and amine added to PdCl2; stirred at 80°C until complete dissolution; powdered K2CO3 (5 equiv.) added; heated (80°C, 5 min); imidazolium salt added; heated with stirring (80°C, 18 h); NaI added; heated (80°C, 30 min); filtered through Celite (CH2Cl2); volatiles removed; purified by flash chromy. (silica gel, hexane in ethyl acetate from 0% to 100% (20 min)); elem. anal.;
DOI:10.1021/om8008475

Reference yield: 81.0%

: 103-83-3
N,N'-dimethylbenzylamine

: 1093348-03-8
1,3-bis(2-tert-butylphenyl)imidazolium chloride

: palladium dichloride

: ITbp-Pd(dmba)Cl

Guidance literature:: N,N'-dimethylbenzylamine; palladium dichloride; In acetonitrile; at 80 ℃; for 0.333333h;

With potassium carbonate; In acetonitrile; for 0.0833333 - 0.166667h;

1,3-bis(2-tert-butylphenyl)imidazolium chloride; In acetonitrile; at 80 ℃; for 18h;