C₃₀H₅₃IO₄Si₂

Base Information

Chemical Name:C₃₀H₅₃IO₄Si₂
CAS No.:1262324-36-6
Molecular Formula:C₃₀H₅₃IO₄Si₂
Molecular Weight:660.824
Hs Code.:

C<sub>30</sub>H<sub>53</sub>IO<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₀H₅₃IO₄Si₂

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Chemical Property of C₃₀H₅₃IO₄Si₂

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Technology Process of C₃₀H₅₃IO₄Si₂

There total 12 articles about C₃₀H₅₃IO₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1262324-70-8
C₃₀H₅₂O₄Si₂

: 1262324-36-6
C₃₀H₅₃IO₄Si₂

Guidance literature:: C₃₀H₅₂O₄Si₂; With Schwartz's reagent; In tetrahydrofuran; at 60 ℃; for 0.5h; Inert atmosphere;

With iodine; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃; for 0.166667h;
DOI:10.1021/jo1019738

Reference yield:

: C₁₆H₃₀O₄Si

: 1262324-36-6
C₃₀H₅₃IO₄Si₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: decane / 180 °C

2.1: decane / 180 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.25 h / 0 - 20 °C / Inert atmosphere

3.2: 0 °C

4.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 13 h / 0 - 20 °C / Inert atmosphere

5.1: 2,6-dimethylpyridine / dichloromethane / 13 h / 20 °C

6.1: Sudan Red B; ozone / methanol; dichloromethane / -78 °C

6.2: -78 - 20 °C / Inert atmosphere

7.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / 0 °C / Inert atmosphere

7.2: 0.75 h / 20 °C

8.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.17 h / -78 - 0 °C / Inert atmosphere

9.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

9.2: 16 h / -78 - 20 °C

10.1: Schwartz's reagent / tetrahydrofuran / 0.5 h / 60 °C / Inert atmosphere

10.2: 0.17 h / 0 - 20 °C

With 2,6-dimethylpyridine; lithium aluminium tetrahydride; Schwartz's reagent; n-butyllithium; Sudan Red B; tetra-(n-butyl)ammonium iodide; sodium hydride; ozone; lithium diisopropyl amide; In tetrahydrofuran; methanol; decane; hexane; dichloromethane; dimethyl sulfoxide; mineral oil; 7.2: Wittig reaction;
DOI:10.1021/jo1019738

Reference yield:

: 1114553-44-4
C₁₅H₃₀O₃Si

: 1262324-36-6
C₃₀H₅₃IO₄Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 13 h / 0 - 20 °C / Inert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / 13 h / 20 °C

3.1: Sudan Red B; ozone / methanol; dichloromethane / -78 °C

3.2: -78 - 20 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / 0 °C / Inert atmosphere

4.2: 0.75 h / 20 °C

5.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.17 h / -78 - 0 °C / Inert atmosphere

6.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

6.2: 16 h / -78 - 20 °C

7.1: Schwartz's reagent / tetrahydrofuran / 0.5 h / 60 °C / Inert atmosphere

7.2: 0.17 h / 0 - 20 °C

With 2,6-dimethylpyridine; Schwartz's reagent; n-butyllithium; Sudan Red B; tetra-(n-butyl)ammonium iodide; sodium hydride; ozone; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane; dichloromethane; dimethyl sulfoxide; mineral oil; 4.2: Wittig reaction;
DOI:10.1021/jo1019738