Quinoxaline, 1-butyl-1,2,3,4-tetrahydro- (6CI)

Base Information

• Chemical Name: Quinoxaline, 1-butyl-1,2,3,4-tetrahydro- (6CI)
• CAS No.: 105105-31-5
• Molecular Formula: C₁₂H₁₈N₂
• Molecular Weight: 190.288
• Hs Code.: 2933990090
• Mol file: 105105-31-5.mol

Synonyms:Quinoxaline, 1-butyl-1,2,3,4-tetrahydro- (6CI);1-BUTYL-1,2,3,4-TETRAHYDROQUINOXALINE

Chemical Property of Quinoxaline, 1-butyl-1,2,3,4-tetrahydro- (6CI)

Chemical Property:

• Boiling Point: 187-191 °C(Press: 21 Torr)
• PKA: 7.98±0.20(Predicted)
• PSA: 15.27000
• Density: 0.981±0.06 g/cm3(Predicted)
• LogP: 2.92160

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Quinoxaline, 1-butyl-1,2,3,4-tetrahydro- (6CI)

There total 2 articles about Quinoxaline, 1-butyl-1,2,3,4-tetrahydro- (6CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-benzenesulfonyl-4-butyl-1,2,3,4-tetrahydro-quinoxaline (7151-42-0) → 1-butyl-1,2,3,4-tetrahydroquinoxaline (105105-31-5)

Guidance literature:

With sulfuric acid;

DOI:10.1021/ja01196a015

Reference yield:

4-butyl-3,4-dihydro-1H-quinoxalin-2-one (73855-48-8) → 1-butyl-1,2,3,4-tetrahydroquinoxaline (105105-31-5)

Guidance literature:

With lithium aluminium tetrahydride; diethyl ether;

DOI:10.1021/jo01084a014

Reference yield: 58.0%

1-butyl-1,2,3,4-tetrahydroquinoxaline (105105-31-5) + C11H5Cl3N2O2 → C23H22Cl2N4O2 (1415407-25-8)

Guidance literature:

With triethylamine; at 20 ℃; for 3h;

DOI:10.1021/jm301071h

upstream raw materials:

4-butyl-3,4-dihydro-1H-quinoxalin-2-one

1-benzenesulfonyl-4-butyl-1,2,3,4-tetrahydro-quinoxaline

Downstream raw materials:

C₂₃H₂₂Cl₂N₄O₂

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