2-[4-(N,N-diphenylamino)phenyl]-5-tributylstannyl-3,4-ethylenedioxythiophene

Base Information

Chemical Name:2-[4-(N,N-diphenylamino)phenyl]-5-tributylstannyl-3,4-ethylenedioxythiophene
CAS No.:1351757-81-7
Molecular Formula:C₃₆H₄₅NO₂SSn
Molecular Weight:674.535
Hs Code.:

Synonyms:2-[4-(N,N-diphenylamino)phenyl]-5-tributylstannyl-3,4-ethylenedioxythiophene

Suppliers and Price of 2-[4-(N,N-diphenylamino)phenyl]-5-tributylstannyl-3,4-ethylenedioxythiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 15 raw suppliers

Chemical Property of 2-[4-(N,N-diphenylamino)phenyl]-5-tributylstannyl-3,4-ethylenedioxythiophene

Chemical Property:

Purity/Quality:: 99% ,98%,Electron Grade , ^*data from raw suppliers

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Technology Process of 2-[4-(N,N-diphenylamino)phenyl]-5-tributylstannyl-3,4-ethylenedioxythiophene

There total 3 articles about 2-[4-(N,N-diphenylamino)phenyl]-5-tributylstannyl-3,4-ethylenedioxythiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1430887-83-4
4-(2,3-dihydrothieno[3,4-b][1,4]dioxin-5-yl)-N,N-diphenylbenzenamine

: 1461-22-9
tributyltin chloride

: 1351757-81-7
2-[4-(N,N-diphenylamino)phenyl]-5-tributylstannyl-3,4-ethylenedioxythiophene

Guidance literature:: 4-(2,3-dihydrothieno[3,4-b][1,4]dioxin-5-yl)-N,N-diphenylbenzenamine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

tributyltin chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.5h;
DOI:10.1016/j.orgel.2016.07.022

Reference yield:

: 36809-26-4
4-N,N-diphenylamino-1-bromobenzene

: 1351757-81-7
2-[4-(N,N-diphenylamino)phenyl]-5-tributylstannyl-3,4-ethylenedioxythiophene

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 12 h / 80 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: 1.5 h / -78 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; 1.1: |Stille Cross Coupling;
DOI:10.1016/j.orgel.2016.07.022

Reference yield:

: 175922-79-9
tributyl(2,3-dihydrothieno[3,4-b][1,4]dioxin-5-yl)-stannane

: 1351757-81-7
2-[4-(N,N-diphenylamino)phenyl]-5-tributylstannyl-3,4-ethylenedioxythiophene

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 12 h / 80 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: 1.5 h / -78 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; 1.1: |Stille Cross Coupling;
DOI:10.1016/j.orgel.2016.07.022