methyl {2-[(2Z)-3-hydroxy-3-(4-methylphenyl)prop-2-enoyl]-4-methylphenyl}-dithiocarbamate

Base Information

Chemical Name:methyl {2-[(2Z)-3-hydroxy-3-(4-methylphenyl)prop-2-enoyl]-4-methylphenyl}-dithiocarbamate
CAS No.:1190084-97-9
Molecular Formula:C₁₉H₁₉NO₂S₂
Molecular Weight:357.497
Hs Code.:

Synonyms:methyl {2-[(2Z)-3-hydroxy-3-(4-methylphenyl)prop-2-enoyl]-4-methylphenyl}-dithiocarbamate

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Chemical Property of methyl {2-[(2Z)-3-hydroxy-3-(4-methylphenyl)prop-2-enoyl]-4-methylphenyl}-dithiocarbamate

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Technology Process of methyl {2-[(2Z)-3-hydroxy-3-(4-methylphenyl)prop-2-enoyl]-4-methylphenyl}-dithiocarbamate

There total 2 articles about methyl {2-[(2Z)-3-hydroxy-3-(4-methylphenyl)prop-2-enoyl]-4-methylphenyl}-dithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1190084-95-7
6-methyl-2-(methylsulfanyl)-4H-3,1-benzothiazin-4-one

: 122-00-9
para-methylacetophenone

: 1190084-97-9
methyl {2-[(2Z)-3-hydroxy-3-(4-methylphenyl)prop-2-enoyl]-4-methylphenyl}-dithiocarbamate

Guidance literature:: para-methylacetophenone; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexanes; at -78 - 0 ℃; Inert atmosphere;

6-methyl-2-(methylsulfanyl)-4H-3,1-benzothiazin-4-one; In tetrahydrofuran; hexanes; at 30 ℃; for 3h;

Reference yield:

: 2941-78-8
2-Amino-5-methylbenzoic acid

: 1190084-97-9
methyl {2-[(2Z)-3-hydroxy-3-(4-methylphenyl)prop-2-enoyl]-4-methylphenyl}-dithiocarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / 1,4-dioxane / 18 h / 5 °C / Inert atmosphere

1.2: 5 °C / Inert atmosphere

2.1: acetic anhydride / 1 h / Reflux

3.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexanes / -78 - 0 °C / Inert atmosphere

3.2: 3 h / 30 °C

With n-butyllithium; acetic anhydride; triethylamine; diisopropylamine; In tetrahydrofuran; 1,4-dioxane; hexanes;