7,9,11-Trimethyl-10-oxo-3-phenyl-2-oxa-6-azatricyclo<5.3.2.0^1,5>dodeca-3,5,8,11-tetraen-4-carbonitril

Base Information

• Chemical Name: 7,9,11-Trimethyl-10-oxo-3-phenyl-2-oxa-6-azatricyclo<5.3.2.0^1,5>dodeca-3,5,8,11-tetraen-4-carbonitril
• CAS No.: 107129-24-8
• Molecular Formula: C₂₀H₁₆N₂O₂
• Molecular Weight: 316.359

Synonyms:7,9,11-Trimethyl-10-oxo-3-phenyl-2-oxa-6-azatricyclo<5.3.2.0^1,5>dodeca-3,5,8,11-tetraen-4-carbonitril

Chemical Property of 7,9,11-Trimethyl-10-oxo-3-phenyl-2-oxa-6-azatricyclo<5.3.2.0^1,5>dodeca-3,5,8,11-tetraen-4-carbonitril

Chemical Property:

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Technology Process of 7,9,11-Trimethyl-10-oxo-3-phenyl-2-oxa-6-azatricyclo<5.3.2.0^1,5>dodeca-3,5,8,11-tetraen-4-carbonitril

There total 3 articles about 7,9,11-Trimethyl-10-oxo-3-phenyl-2-oxa-6-azatricyclo<5.3.2.0^1,5>dodeca-3,5,8,11-tetraen-4-carbonitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

<α-(2,4,6-Trimethyl-7-oxo-1,3,5-cycloheptatrien-1-yloxy)benzyliden>propandinitril (107129-17-9) → 7,9,11-Trimethyl-10-oxo-3-phenyl-2-oxa-6-azatricyclo<5.3.2.01,5>dodeca-3,5,8,11-tetraen-4-carbonitril (107129-24-8)

Guidance literature:

In toluene; at 110 ℃; for 0.0833333h;

Reference yield:

3,5,7-trimethyltropolone (2885-58-7) → 7,9,11-Trimethyl-10-oxo-3-phenyl-2-oxa-6-azatricyclo<5.3.2.01,5>dodeca-3,5,8,11-tetraen-4-carbonitril (107129-24-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 57 percent / Et₃N, DMAP / CH₂Cl₂ / 0.25 h

2: 95 percent / toluene / 0.08 h / 110 °C

With dmap; triethylamine; In dichloromethane; toluene;

Reference yield:

2-cyano-3-chlorocinnamonitrile (18270-61-6) → 7,9,11-Trimethyl-10-oxo-3-phenyl-2-oxa-6-azatricyclo<5.3.2.01,5>dodeca-3,5,8,11-tetraen-4-carbonitril (107129-24-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 57 percent / Et₃N, DMAP / CH₂Cl₂ / 0.25 h

2: 95 percent / toluene / 0.08 h / 110 °C

With dmap; triethylamine; In dichloromethane; toluene;

upstream raw materials:

<α-(2,4,6-Trimethyl-7-oxo-1,3,5-cycloheptatrien-1-yloxy)benzyliden>propandinitril

3,5,7-trimethyltropolone

2-cyano-3-chlorocinnamonitrile

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