6-(tert-Butyl-diphenyl-silanyloxymethyl)-6,7-dihydro-5H-[1,3]dithiolo[4,5-b][1,4]dithiepine-2-thione

Base Information

Chemical Name:6-(tert-Butyl-diphenyl-silanyloxymethyl)-6,7-dihydro-5H-[1,3]dithiolo[4,5-b][1,4]dithiepine-2-thione
CAS No.:209917-58-8
Molecular Formula:C₂₃H₂₆OS₅Si
Molecular Weight:506.874
Hs Code.:

Synonyms:6-(tert-Butyl-diphenyl-silanyloxymethyl)-6,7-dihydro-5H-[1,3]dithiolo[4,5-b][1,4]dithiepine-2-thione

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Chemical Property of 6-(tert-Butyl-diphenyl-silanyloxymethyl)-6,7-dihydro-5H-[1,3]dithiolo[4,5-b][1,4]dithiepine-2-thione

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Technology Process of 6-(tert-Butyl-diphenyl-silanyloxymethyl)-6,7-dihydro-5H-[1,3]dithiolo[4,5-b][1,4]dithiepine-2-thione

There total 1 articles about 6-(tert-Butyl-diphenyl-silanyloxymethyl)-6,7-dihydro-5H-[1,3]dithiolo[4,5-b][1,4]dithiepine-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 209917-57-7
6-Hydroxymethyl-6,7-dihydro-5H-[1,3]dithiolo[4,5-b][1,4]dithiepine-2-thione

: 209917-58-8
6-(tert-Butyl-diphenyl-silanyloxymethyl)-6,7-dihydro-5H-[1,3]dithiolo[4,5-b][1,4]dithiepine-2-thione

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 18h;
DOI:10.1039/a800225h

Reference yield: 88.0%

: 209917-58-8
6-(tert-Butyl-diphenyl-silanyloxymethyl)-6,7-dihydro-5H-[1,3]dithiolo[4,5-b][1,4]dithiepine-2-thione

: 209917-59-9
6-(tert-Butyl-diphenyl-silanyloxymethyl)-6,7-dihydro-5H-[1,3]dithiolo[4,5-b][1,4]dithiepin-2-one

Guidance literature:: With mercury(II) diacetate; acetic acid; In chloroform; at 20 ℃; for 18h;
DOI:10.1039/a800225h

Reference yield:

: 209917-58-8
6-(tert-Butyl-diphenyl-silanyloxymethyl)-6,7-dihydro-5H-[1,3]dithiolo[4,5-b][1,4]dithiepine-2-thione

: 209917-60-2
[2-(4,5-Bis-methylsulfanyl-[1,3]dithiol-2-ylidene)-6,7-dihydro-5H-[1,3]dithiolo[4,5-b][1,4]dithiepin-6-ylmethoxy]-tert-butyl-diphenyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / mercuric acetate, AcOH / CHCl₃ / 18 h / 20 °C

2: triethyl phosphite / 2 h / 130 °C

With mercury(II) diacetate; acetic acid; triethyl phosphite; In chloroform;
DOI:10.1039/a800225h