4-O-<3-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl>-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl bromide

Base Information

Chemical Name:4-O-<3-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl>-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl bromide
CAS No.:127529-85-5
Molecular Formula:C₅₉H₆₅BrN₆O₁₆
Molecular Weight:1194.1
Hs Code.:

4-O-<3-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl>-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl bromide

Synonyms:4-O-<3-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl>-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl bromide

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Chemical Property of 4-O-<3-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl>-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl bromide

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Technology Process of 4-O-<3-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl>-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl bromide

There total 3 articles about 4-O-<3-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl>-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-O-<3-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl>-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α/β-D-glucopyranose

: 127529-85-5
4-O-<3-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl>-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl bromide

Guidance literature:: With N-(bromomethylene)-N-methylmethanaminium bromide;
DOI:10.1016/S0040-4020(01)88221-1

Reference yield:

: 127529-67-3
4-O-<3-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl>-1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose

: 127529-85-5
4-O-<3-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl>-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / acetic acid / trifluoroacetic acid / 3 h / 0 - 20 °C

2: 84 percent / piperidine / tetrahydrofuran / 20 h

3: oxalyl bromide / dimethylformamide; CHCl₃ / 2 h / 0 - 20 °C

With piperidine; Oxalyl bromide; acetic acid; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide; trifluoroacetic acid;

Reference yield:

: 4-O-<3-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl>-1,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α/β-D-glucopyranose

: 127529-85-5
4-O-<3-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-2,4-di-O-benzyl-β-D-galactopyranosyl>-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / piperidine / tetrahydrofuran / 20 h

2: oxalyl bromide / dimethylformamide; CHCl₃ / 2 h / 0 - 20 °C

With piperidine; Oxalyl bromide; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;