[((C₆H₅)2PCH₂P(C₆H₅)2)2Pt₂Cl₂CH₃]⁽¹⁺⁾*SbF₆^(1-)=[((C₆H₅)2PCH₂P(C₆H₅)2)2Pt₂Cl₂CH₃]SbF₆

Base Information

• Chemical Name: [((C₆H₅)2PCH₂P(C₆H₅)2)2Pt₂Cl₂CH₃]⁽¹⁺⁾*SbF₆^(1-)=[((C₆H₅)2PCH₂P(C₆H₅)2)2Pt₂Cl₂CH₃]SbF₆
• CAS No.: 86802-73-5
• Molecular Formula: C₅₁H₄₇Cl₂P₄Pt₂*F₆Sb
• Molecular Weight: 1480.64

Synonyms:[((C₆H₅)2PCH₂P(C₆H₅)2)2Pt₂Cl₂CH₃]⁽¹⁺⁾*SbF₆^(1-)=[((C₆H₅)2PCH₂P(C₆H₅)2)2Pt₂Cl₂CH₃]SbF₆

Chemical Property of [((C₆H₅)2PCH₂P(C₆H₅)2)2Pt₂Cl₂CH₃]⁽¹⁺⁾*SbF₆^(1-)=[((C₆H₅)2PCH₂P(C₆H₅)2)2Pt₂Cl₂CH₃]SbF₆

Chemical Property:

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Technology Process of [((C₆H₅)2PCH₂P(C₆H₅)2)2Pt₂Cl₂CH₃]⁽¹⁺⁾*SbF₆^(1-)=[((C₆H₅)2PCH₂P(C₆H₅)2)2Pt₂Cl₂CH₃]SbF₆

There total 2 articles about [((C₆H₅)2PCH₂P(C₆H₅)2)2Pt₂Cl₂CH₃]⁽¹⁺⁾*SbF₆^(1-)=[((C₆H₅)2PCH₂P(C₆H₅)2)2Pt₂Cl₂CH₃]SbF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

Pt2Cl2CH2((C6H5)4P2CH2)2 (68851-49-0) + hexafluoro antimony(V)acid hexahydrate → [((C6H5)2PCH2P(C6H5)2)2Pt2Cl2CH3](1+)*SbF6(1-)=[((C6H5)2PCH2P(C6H5)2)2Pt2Cl2CH3]SbF6 (86802-73-5)

Guidance literature:

In dichloromethane; to HSbF6*6H2O added suspn. of Pt complex (1 equiv) in CH2Cl2, stirred at room temp. under N2 for 2.25 h; concd., pptd. by addn. of Et2O; elem. anal.;

Reference yield:

hexafluoroantimonic acid + Pt2Cl2CH2((C6H5)4P2CH2)2 (68851-49-0) → [((C6H5)2PCH2P(C6H5)2)2Pt2Cl2CH3](1+)*SbF6(1-)=[((C6H5)2PCH2P(C6H5)2)2Pt2Cl2CH3]SbF6 (86802-73-5)

Guidance literature:

In not given;

DOI:10.1016/S0022-328X(00)85863-5

Reference yield: 96.0%

sodium tetrahydroborate (16940-66-2) + [((C6H5)2PCH2P(C6H5)2)2Pt2Cl2CH3](1+)*SbF6(1-)=[((C6H5)2PCH2P(C6H5)2)2Pt2Cl2CH3]SbF6 (86802-73-5) → {Pt2H2(CH3)((C6H5)2PCH2P(C6H5)2)2}(1+)*SbF6(1-)={Pt2H2(CH3)((C6H5)2PCH2P(C6H5)2)2}SbF6 (86802-75-7)

Guidance literature:

In methanol; dichloromethane; soln. of NaBH4 in MeOH added to soln. of Pt complex in CH2Cl2, stirred under N2 in dark at room temp. for 30 min; evapd., dried in vac., extd. with CH2Cl2, concd., pptd. by addn. of Et2O; elem. anal.;

upstream raw materials:

Pt₂Cl₂CH₂((C₆H₅)4P₂CH₂)2

Downstream raw materials:

{Pt₂H₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)2}⁽¹⁺⁾*SbF₆^(1-)={Pt₂H₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)2}SbF₆

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