methyl 3-((1r,4r)-4-(4-(trifluoromethylsulfonyloxy)phenyl)cyclohexyl)propanoate

Base Information

Chemical Name:methyl 3-((1r,4r)-4-(4-(trifluoromethylsulfonyloxy)phenyl)cyclohexyl)propanoate
CAS No.:1166828-54-1
Molecular Formula:C₁₇H₂₁F₃O₅S
Molecular Weight:394.412
Hs Code.:

Synonyms:methyl 3-((1r,4r)-4-(4-(trifluoromethylsulfonyloxy)phenyl)cyclohexyl)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-((1r,4r)-4-(4-(trifluoromethylsulfonyloxy)phenyl)cyclohexyl)propanoate

Chemical Property:

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Technology Process of methyl 3-((1r,4r)-4-(4-(trifluoromethylsulfonyloxy)phenyl)cyclohexyl)propanoate

There total 3 articles about methyl 3-((1r,4r)-4-(4-(trifluoromethylsulfonyloxy)phenyl)cyclohexyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1166828-56-3
methyl 3-((1r,4r)-4-(4-hydroxyphenyl)cyclohexyl)propanoate

: 1166828-54-1
methyl 3-((1r,4r)-4-(4-(trifluoromethylsulfonyloxy)phenyl)cyclohexyl)propanoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 1155663-17-4
3-((1r,4r)-4-(4-hydroxyphenyl)cyclohexyl)propanoic acid

: 1166828-54-1
methyl 3-((1r,4r)-4-(4-(trifluoromethylsulfonyloxy)phenyl)cyclohexyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 3 h / 70 °C

2: triethylamine / dichloromethane / 0 - 20 °C

With sulfuric acid; triethylamine; In dichloromethane;

Reference yield:

: 1166828-60-9
4-((1r,4r)-4-(2-cyanoethyl)cyclohexyl)phenyl methanesulfonate

: 1166828-54-1
methyl 3-((1r,4r)-4-(4-(trifluoromethylsulfonyloxy)phenyl)cyclohexyl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; sodium hydroxide / propylene glycol / 1 h / 140 °C

1.2: pH 2

2.1: sulfuric acid / 3 h / 70 °C

3.1: triethylamine / dichloromethane / 0 - 20 °C

With sulfuric acid; water; triethylamine; sodium hydroxide; In propylene glycol; dichloromethane;