[3-ethyl-4-(1-methyl-1H-imidazo[4,5-c]pyridin-6-ylamino)phenyl]acetonitrile

Base Information

Chemical Name:[3-ethyl-4-(1-methyl-1H-imidazo[4,5-c]pyridin-6-ylamino)phenyl]acetonitrile
CAS No.:1449514-98-0
Molecular Formula:C₁₇H₁₇N₅
Molecular Weight:291.355
Hs Code.:

Synonyms:[3-ethyl-4-(1-methyl-1H-imidazo[4,5-c]pyridin-6-ylamino)phenyl]acetonitrile

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Chemical Property of [3-ethyl-4-(1-methyl-1H-imidazo[4,5-c]pyridin-6-ylamino)phenyl]acetonitrile

Chemical Property:

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Technology Process of [3-ethyl-4-(1-methyl-1H-imidazo[4,5-c]pyridin-6-ylamino)phenyl]acetonitrile

There total 4 articles about [3-ethyl-4-(1-methyl-1H-imidazo[4,5-c]pyridin-6-ylamino)phenyl]acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 607373-83-1
2-chloro-4-methoxy-5-nitro-pyridine

: 1449514-98-0
[3-ethyl-4-(1-methyl-1H-imidazo[4,5-c]pyridin-6-ylamino)phenyl]acetonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 2 h / 20 °C

2: iron; acetic acid / 50 - 80 °C

3: orthoformic acid triethyl ester / 4 h / 100 °C

4: palladium diacetate; caesium carbonate; XPhos / toluene / 16 h / 100 °C

With palladium diacetate; iron; caesium carbonate; acetic acid; orthoformic acid triethyl ester; XPhos; In tetrahydrofuran; toluene;

Reference yield:

: 882855-96-1
2-(4-amino-3-bromophenyl)acetonitrile

: 1449514-98-0
[3-ethyl-4-(1-methyl-1H-imidazo[4,5-c]pyridin-6-ylamino)phenyl]acetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; caesium carbonate / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 55 °C / Inert atmosphere

2: palladium diacetate; caesium carbonate; XPhos / toluene / 16 h / 100 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; palladium diacetate; caesium carbonate; XPhos; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;

Reference yield:

: 87034-76-2
6-chloro-N⁴-methylpyridine-3,4-diamine

: 1449514-98-0
[3-ethyl-4-(1-methyl-1H-imidazo[4,5-c]pyridin-6-ylamino)phenyl]acetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: orthoformic acid triethyl ester / 4 h / 100 °C

2: palladium diacetate; caesium carbonate; XPhos / toluene / 16 h / 100 °C

With palladium diacetate; caesium carbonate; orthoformic acid triethyl ester; XPhos; In toluene;