meso-1,2-Bis(3-methoxyphenyl)ethylenediamine

Base Information

• Chemical Name: meso-1,2-Bis(3-methoxyphenyl)ethylenediamine
• CAS No.: 763081-88-5
• Molecular Formula: C₁₆H₂₀N₂O₂
• Molecular Weight: 272.347

Synonyms:meso-1,2-Bis(3-methoxyphenyl)ethylenediamine

Chemical Property of meso-1,2-Bis(3-methoxyphenyl)ethylenediamine

Chemical Property:

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Technology Process of meso-1,2-Bis(3-methoxyphenyl)ethylenediamine

There total 4 articles about meso-1,2-Bis(3-methoxyphenyl)ethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

3-methoxy-benzaldehyde (591-31-1) → meso-1,2-Bis(3-methoxyphenyl)ethylenediamine (763081-88-5)

Guidance literature:

With tris(bipyridine)ruthenium(II) dichloride hexahydrate; ammonia; N-ethyl-N,N-diisopropylamine; scandium tris(trifluoromethanesulfonate); In methanol; acetonitrile; at 0 - 25 ℃; for 15h; chemoselective reaction; Sealed tube; Inert atmosphere; Irradiation;

DOI:10.1021/acs.orglett.8b01637

Reference yield: 75.0%

N,N'-Disalicylidene-meso-1,2-bis(3-methoxyphenyl)ethylenediamine → meso-1,2-Bis(3-methoxyphenyl)ethylenediamine (763081-88-5)

Guidance literature:

With sulfuric acid;

DOI:10.1002/ardp.19893220107

Reference yield:

N,N'-Disalicylidene-meso-1,2-bis(3-methoxyphenyl)ethylenediamine → meso-1,2-Bis(3-methoxyphenyl)ethylenediamine (763081-88-5) + d,l-1,2-diamino-1,2-bis(3-methoxyphenyl)ethane

Guidance literature:

With sulfuric acid; Yield given. Multistep reaction; 1.) 210-220 deg C, 10 min, 2.) heating;

DOI:10.1002/ardp.19893220107

upstream raw materials:

3-methoxy-benzaldehyde

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