Technology Process of C23H26N2O6
There total 6 articles about C23H26N2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C23H24N2O8;
With
acetic acid; zinc;
In
ethanol;
for 0.0833333h;
Reflux;
With
sodium hydrogencarbonate;
In
water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: trichloroisocyanuric acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0 °C
2: 2,6-dimethylpyridine / dichloromethane / 1 h / -45 - 40 °C / Inert atmosphere
3: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / Inert atmosphere
4: lithium borohydride; ethanol / tetrahydrofuran / 1 h / 15 - 25 °C / Cooling with ice
5: zinc; acetic acid / ethanol / 0.08 h / Reflux
With
2,6-dimethylpyridine; lithium borohydride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; ethanol; trichloroisocyanuric acid; sodium carbonate; acetic acid; zinc;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; ethanol; dichloromethane; water; toluene;
3: Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 2,6-dimethylpyridine / dichloromethane / 1 h / -45 - 40 °C / Inert atmosphere
2: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / Inert atmosphere
3: lithium borohydride; ethanol / tetrahydrofuran / 1 h / 15 - 25 °C / Cooling with ice
4: zinc; acetic acid / ethanol / 0.08 h / Reflux
With
2,6-dimethylpyridine; lithium borohydride; ethanol; sodium carbonate; acetic acid; zinc;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; ethanol; dichloromethane; water; toluene;
2: Suzuki Coupling;