2,2',2'',3,3',3''-hexahydroxy-4,4',4''-<1,3,5-benzenetriyltris(4,1-phenylenmethyleniminocarbonyl)>tris benzoic acid

Base Information

Chemical Name:2,2',2'',3,3',3''-hexahydroxy-4,4',4''-<1,3,5-benzenetriyltris(4,1-phenylenmethyleniminocarbonyl)>tris benzoic acid
CAS No.:112994-54-4
Molecular Formula:C₅₁H₃₉N₃O₁₅
Molecular Weight:933.882
Hs Code.:

Synonyms:2,2',2'',3,3',3''-hexahydroxy-4,4',4''-<1,3,5-benzenetriyltris(4,1-phenylenmethyleniminocarbonyl)>tris benzoic acid

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Chemical Property of 2,2',2'',3,3',3''-hexahydroxy-4,4',4''-<1,3,5-benzenetriyltris(4,1-phenylenmethyleniminocarbonyl)>tris benzoic acid

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Technology Process of 2,2',2'',3,3',3''-hexahydroxy-4,4',4''-<1,3,5-benzenetriyltris(4,1-phenylenmethyleniminocarbonyl)>tris benzoic acid

There total 2 articles about 2,2',2'',3,3',3''-hexahydroxy-4,4',4''-<1,3,5-benzenetriyltris(4,1-phenylenmethyleniminocarbonyl)>tris benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 112994-48-6
trimethyl-2,2',2'',3,3',3''-hexamethoxy-4,4',4''-<1,3,5-benzenetriyltris-(4,1-phenylenmethyleniminocarbonyl)>tris benzoate

: 112994-54-4
2,2',2'',3,3',3''-hexahydroxy-4,4',4''-<1,3,5-benzenetriyltris(4,1-phenylenmethyleniminocarbonyl)>tris benzoic acid

Guidance literature:: With boron tribromide; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1016/S0040-4020(01)86788-0

Reference yield:

: 112994-46-4
C₂₇H₂₇N₃

: 112994-54-4
2,2',2'',3,3',3''-hexahydroxy-4,4',4''-<1,3,5-benzenetriyltris(4,1-phenylenmethyleniminocarbonyl)>tris benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / N,N-dimethyl-acetamide / 4 h

2: 81 percent / BBr₃ / CH₂Cl₂ / 24 h / Ambient temperature

With boron tribromide; triethylamine; In dichloromethane; N,N-dimethyl acetamide;
DOI:10.1016/S0040-4020(01)86788-0