6H,12H-5,11-methanodibenzo[b,f][1,5]diazocine-2,8-diylacetic acid pentafluorophenyl ester

Base Information

Chemical Name:6H,12H-5,11-methanodibenzo[b,f][1,5]diazocine-2,8-diylacetic acid pentafluorophenyl ester
CAS No.:442685-97-4
Molecular Formula:C₃₁H₁₆F₁₀N₂O₄
Molecular Weight:670.463
Hs Code.:

Synonyms:6H,12H-5,11-methanodibenzo[b,f][1,5]diazocine-2,8-diylacetic acid pentafluorophenyl ester

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Chemical Property of 6H,12H-5,11-methanodibenzo[b,f][1,5]diazocine-2,8-diylacetic acid pentafluorophenyl ester

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Technology Process of 6H,12H-5,11-methanodibenzo[b,f][1,5]diazocine-2,8-diylacetic acid pentafluorophenyl ester

There total 3 articles about 6H,12H-5,11-methanodibenzo[b,f][1,5]diazocine-2,8-diylacetic acid pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 442685-96-3
2,8-bis(hydroxycarbonylmethyl)-6H,12H-5,11-methanodibenzo[b,f][1,5]diazocine

: 442685-97-4
6H,12H-5,11-methanodibenzo[b,f][1,5]diazocine-2,8-diylacetic acid pentafluorophenyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 12h;
DOI:10.3987/COM-01-9409

Reference yield:

: 39552-81-3
methyl p-aminophenylacetate

: 442685-97-4
6H,12H-5,11-methanodibenzo[b,f][1,5]diazocine-2,8-diylacetic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / trifluoroacetic acid / 48 h / 20 °C

2: 95 percent / LiOH*H₂O / methanol; H₂O / 24 h / 20 °C

3: 97 percent / DCC / CH₂Cl₂ / 12 h / 20 °C

With lithium hydroxide; dicyclohexyl-carbodiimide; In methanol; dichloromethane; water; trifluoroacetic acid;
DOI:10.3987/COM-01-9409

Reference yield:

: 144243-02-7,167934-94-3
2,8-bis(2-methoxycarbonylmethyl)-6H,12H-5,11-methano-dibenzo<1,5>diazocine

: 442685-97-4
6H,12H-5,11-methanodibenzo[b,f][1,5]diazocine-2,8-diylacetic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / LiOH*H₂O / methanol; H₂O / 24 h / 20 °C

2: 97 percent / DCC / CH₂Cl₂ / 12 h / 20 °C

With lithium hydroxide; dicyclohexyl-carbodiimide; In methanol; dichloromethane; water;
DOI:10.3987/COM-01-9409