5,6-Dimethyl-7-(1-methyl-2-phenylethenyl)-7H-pyrrolo<2,3-d>pyrimidin-4-amin

Base Information

Chemical Name:5,6-Dimethyl-7-(1-methyl-2-phenylethenyl)-7H-pyrrolo<2,3-d>pyrimidin-4-amin
CAS No.:103026-54-6
Molecular Formula:C₁₇H₁₈N₄
Molecular Weight:278.357
Hs Code.:

Synonyms:5,6-Dimethyl-7-(1-methyl-2-phenylethenyl)-7H-pyrrolo<2,3-d>pyrimidin-4-amin

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Chemical Property of 5,6-Dimethyl-7-(1-methyl-2-phenylethenyl)-7H-pyrrolo<2,3-d>pyrimidin-4-amin

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Technology Process of 5,6-Dimethyl-7-(1-methyl-2-phenylethenyl)-7H-pyrrolo<2,3-d>pyrimidin-4-amin

There total 3 articles about 5,6-Dimethyl-7-(1-methyl-2-phenylethenyl)-7H-pyrrolo<2,3-d>pyrimidin-4-amin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.5%

: 103026-50-2
7-(2-Hydroxy-1-methyl-2-phenylethyl)-5,6-dimethyl-7H-pyrrolo<2,3-d>pyrimidin-4-amin

: 103026-54-6
5,6-Dimethyl-7-(1-methyl-2-phenylethenyl)-7H-pyrrolo<2,3-d>pyrimidin-4-amin

Guidance literature:: With PPA; at 60 ℃; for 4h;

Reference yield:

: 48115-38-4,58550-13-3,757124-50-8
norepinephrine

: 103026-54-6
5,6-Dimethyl-7-(1-methyl-2-phenylethenyl)-7H-pyrrolo<2,3-d>pyrimidin-4-amin

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) p-toluenesulfonic acid / 1.) toluene, reflux

2: 83.6 percent / 85percent formic acid, DMF / 8 h / Heating

3: 84.5 percent / polyphosphoric acid / 4 h / 60 °C

With formic acid; PPA; toluene-4-sulfonic acid; N,N-dimethyl-formamide;

Reference yield:

: 103026-09-1
2-Amino-1-(2-hydroxy-1-methyl-2-phenylethyl)-4,5-dimethyl-3-pyrrolcarbonitril

: 103026-54-6
5,6-Dimethyl-7-(1-methyl-2-phenylethenyl)-7H-pyrrolo<2,3-d>pyrimidin-4-amin

Guidance literature:: Multi-step reaction with 2 steps

1: 83.6 percent / 85percent formic acid, DMF / 8 h / Heating

2: 84.5 percent / polyphosphoric acid / 4 h / 60 °C

With formic acid; PPA; N,N-dimethyl-formamide;