macrocycle 1a

Base Information

Chemical Name:macrocycle 1a
CAS No.:1155917-95-5
Molecular Formula:C₄₈H₄₅N₃O₉
Molecular Weight:807.9
Hs Code.:

Synonyms:macrocycle 1a

Suppliers and Price of macrocycle 1a

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of macrocycle 1a

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of macrocycle 1a

There total 5 articles about macrocycle 1a which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1155918-00-5
4-(N-(2,4-dimethoxybenzyl)-4-(N-(2,4-dimethoxybenzyl)-4-(2,4-dimethoxybenzylamino)benzamido)benzamido)benzoic acid

: 1155917-95-5
macrocycle 1a

Guidance literature:: With sodium hydrogencarbonate; dichlorotriphenylphosphorane; In chloroform; for 20h; Reflux; Inert atmosphere;
DOI:10.1016/j.tetlet.2009.02.186

Reference yield: 33.0%

: phenyl 4-((2,4-dimethoxybenzyl)amino)benzoate

: 1155917-95-5
macrocycle 1a

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at 20 ℃; for 18h;
DOI:10.1021/ja506646s

Reference yield:

: C₂₂H₁₉NO₄

: 1155917-95-5
macrocycle 1a

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / tetrahydrofuran; methanol / 18 h / Cooling with ice

2: lithium hexamethyldisilazane / tetrahydrofuran / 18 h / 20 °C

With sodium tetrahydroborate; lithium hexamethyldisilazane; In tetrahydrofuran; methanol;
DOI:10.1021/ja506646s