(3,4-dichlorophenoxy)methyl 2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl methyl phosphate

Base Information

Chemical Name:(3,4-dichlorophenoxy)methyl 2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl methyl phosphate
CAS No.:174867-52-8
Molecular Formula:C₂₆H₂₉Cl₂O₇P
Molecular Weight:555.392
Hs Code.:

Synonyms:(3,4-dichlorophenoxy)methyl 2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl methyl phosphate

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Chemical Property of (3,4-dichlorophenoxy)methyl 2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl methyl phosphate

Chemical Property:

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Technology Process of (3,4-dichlorophenoxy)methyl 2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl methyl phosphate

There total 6 articles about (3,4-dichlorophenoxy)methyl 2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl methyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 94637-84-0
3,4-dichlorophenoxymethylene chloride

: tert-butylammonium 2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl methyl phosphate

: 174867-52-8
(3,4-dichlorophenoxy)methyl 2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl methyl phosphate

Guidance literature:: With silver(l) oxide; In acetonitrile; at 50 ℃; for 48h;

Reference yield:

: 6627-55-0
2-bromo-p-cresol

: 174867-52-8
(3,4-dichlorophenoxy)methyl 2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl methyl phosphate

Guidance literature:: Multi-step reaction with 7 steps

1: 65 percent / n-BuLi / hexane; diethyl ether / 1.) room temperature, 2 h, 2.) -78 deg C -> 0 deg C, 1 h

2: 70 percent / N,N-diisopropylethylamine / dimethylformamide

3: 80 percent / N,N-diisopropylethylamine / tetrahydrofuran / 72 h

4: 94 percent / Bu₄NF / tetrahydrofuran / 0.25 h

5: 1.) N,N-diisopropylethylamine, 3.) I₂, pyridine / 1.) THF, -78 deg C, 5 min; 0 deg C, 100 min, 2.) -78 deg C, 1 h, 3.) THF, H₂O, room temperature, 5 min

6: 46 °C

7: 63 percent / Ag₂O / acetonitrile / 48 h / 50 °C

With pyridine; n-butyllithium; tetrabutyl ammonium fluoride; iodine; N-ethyl-N,N-diisopropylamine; silver(l) oxide; In tetrahydrofuran; diethyl ether; hexane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 174867-46-0
2-(1-hydroxy-1-methylethyl)-4-methylphenyl tert-butyldimethylsilylether

: 174867-52-8
(3,4-dichlorophenoxy)methyl 2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl methyl phosphate

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / N,N-diisopropylethylamine / tetrahydrofuran / 72 h

2: 94 percent / Bu₄NF / tetrahydrofuran / 0.25 h

3: 1.) N,N-diisopropylethylamine, 3.) I₂, pyridine / 1.) THF, -78 deg C, 5 min; 0 deg C, 100 min, 2.) -78 deg C, 1 h, 3.) THF, H₂O, room temperature, 5 min

4: 46 °C

5: 63 percent / Ag₂O / acetonitrile / 48 h / 50 °C

With pyridine; tetrabutyl ammonium fluoride; iodine; N-ethyl-N,N-diisopropylamine; silver(l) oxide; In tetrahydrofuran; acetonitrile;