2-(4-methoxyphenyl)-4-phenyl-8-<2-(4-methoxyphenyl)-4-phenyl-6,7-dihydro-5H-1-benzo-8-thiopyranyl>-6,7-dihydro-5H-1-benzothiopyran

Base Information

• Chemical Name: 2-(4-methoxyphenyl)-4-phenyl-8-<2-(4-methoxyphenyl)-4-phenyl-6,7-dihydro-5H-1-benzo-8-thiopyranyl>-6,7-dihydro-5H-1-benzothiopyran
• CAS No.: 114056-99-4
• Molecular Formula: C₄₄H₃₈O₂S₂
• Molecular Weight: 662.917

Synonyms:2-(4-methoxyphenyl)-4-phenyl-8-<2-(4-methoxyphenyl)-4-phenyl-6,7-dihydro-5H-1-benzo-8-thiopyranyl>-6,7-dihydro-5H-1-benzothiopyran

Chemical Property of 2-(4-methoxyphenyl)-4-phenyl-8-<2-(4-methoxyphenyl)-4-phenyl-6,7-dihydro-5H-1-benzo-8-thiopyranyl>-6,7-dihydro-5H-1-benzothiopyran

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Technology Process of 2-(4-methoxyphenyl)-4-phenyl-8-<2-(4-methoxyphenyl)-4-phenyl-6,7-dihydro-5H-1-benzo-8-thiopyranyl>-6,7-dihydro-5H-1-benzothiopyran

There total 4 articles about 2-(4-methoxyphenyl)-4-phenyl-8-<2-(4-methoxyphenyl)-4-phenyl-6,7-dihydro-5H-1-benzo-8-thiopyranyl>-6,7-dihydro-5H-1-benzothiopyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2-(4-Methoxyphenyl)-4-phenylcyclohexathiopyrylium Tetrafluoroborate → 2-(4-methoxyphenyl)-4-phenyl-8-<2-(4-methoxyphenyl)-4-phenyl-6,7-dihydro-5H-1-benzo-8-thiopyranyl>-6,7-dihydro-5H-1-benzothiopyran (114056-99-4)

Guidance literature:

With sodium hydroxide; potassium hexacyanoferrate(III); In ethanol; water; at 50 ℃; for 1.5h;

Reference yield: 50.0%

4-phenyl-2-(p-methoxyphenyl)cyclohexathiopyrylium tetrafluoroborate → 2-(4-methoxyphenyl)-4-phenyl-8-<2-(4-methoxyphenyl)-4-phenyl-6,7-dihydro-5H-1-benzo-8-thiopyranyl>-6,7-dihydro-5H-1-benzothiopyran (114056-99-4)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 48h;

DOI:10.1007/BF00529472

Reference yield: 34.0%

2-(4-Methoxyphenyl)-4-phenylcyclohexathiopyrylium Tetrafluoroborate + 2-(4-Methoxyphenyl)-4-phenyl-4H-cyclohexathiopyran (94594-87-3) → 2-(4-methoxyphenyl)-4-phenyl-8-<2-(4-methoxyphenyl)-4-phenyl-6,7-dihydro-5H-1-benzo-8-thiopyranyl>-6,7-dihydro-5H-1-benzothiopyran (114056-99-4)

Guidance literature:

In acetonitrile; at 50 ℃; for 6h;

DOI:10.1007/BF00529371

upstream raw materials:

2-(4-Methoxyphenyl)-4-phenyl-4H-cyclohexathiopyran

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