(2S)-6-benzyloxy-2-(3-(tert-butoxycarbonylamino)propyl)-3-(hydroxymethyl)-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline ⁽¹³⁾

Base Information

• Chemical Name: (2S)-6-benzyloxy-2-(3-(tert-butoxycarbonylamino)propyl)-3-(hydroxymethyl)-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline ⁽¹³⁾
• CAS No.: 1100289-08-4
• Molecular Formula: C₃₂H₃₈N₂O₆S
• Molecular Weight: 578.73

Synonyms:(2S)-6-benzyloxy-2-(3-(tert-butoxycarbonylamino)propyl)-3-(hydroxymethyl)-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline ⁽¹³⁾

Chemical Property of (2S)-6-benzyloxy-2-(3-(tert-butoxycarbonylamino)propyl)-3-(hydroxymethyl)-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline ⁽¹³⁾

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Technology Process of (2S)-6-benzyloxy-2-(3-(tert-butoxycarbonylamino)propyl)-3-(hydroxymethyl)-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline ⁽¹³⁾

There total 1 articles about (2S)-6-benzyloxy-2-(3-(tert-butoxycarbonylamino)propyl)-3-(hydroxymethyl)-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline ⁽¹³⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(2S)-6-benzyloxy-2-(3-(tert-butoxycarbonylamino)propyl)-3-formyl-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline (13) (1100289-54-0) → (2S)-6-benzyloxy-2-(3-(tert-butoxycarbonylamino)propyl)-3-(hydroxymethyl)-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline (13) (1100289-08-4)

Guidance literature:

With sodium tetrahydroborate; cerium(III) chloride heptahydrate; In acetonitrile; at 20 ℃; for 18h;

DOI:10.1016/j.tet.2008.10.032

Reference yield: 81.5%

(2S)-6-benzyloxy-2-(3-(tert-butoxycarbonylamino)propyl)-3-(hydroxymethyl)-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline (13) (1100289-08-4) → {3-[6-benzyloxy-1a-hydroxymethyl-3-(toluene-4-sulfonyl)-1a,2,3,7b-tetrahydro-1-oxa-3-azacyclopropa[a]naphthalen-2-yl]-propyl}-carbamic acid tert-butyl ester (1100289-10-8)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.tet.2008.10.032

upstream raw materials:

(2S)-6-benzyloxy-2-(3-(tert-butoxycarbonylamino)propyl)-3-formyl-1-(toluene-4-sulfonyl)-1,2-dihydroquinoline ⁽¹³⁾

Downstream raw materials:

{3-[6-benzyloxy-1a-hydroxymethyl-3-(toluene-4-sulfonyl)-1a,2,3,7b-tetrahydro-1-oxa-3-azacyclopropa[a]naphthalen-2-yl]-propyl}-carbamic acid tert-butyl ester

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