C₃₄H₅₆INO₇Si

Base Information

Chemical Name:C₃₄H₅₆INO₇Si
CAS No.:1378889-91-8
Molecular Formula:C₃₄H₅₆INO₇Si
Molecular Weight:745.811
Hs Code.:

C<sub>34</sub>H<sub>56</sub>INO<sub>7</sub>Si

Synonyms:C₃₄H₅₆INO₇Si

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Chemical Property of C₃₄H₅₆INO₇Si

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Technology Process of C₃₄H₅₆INO₇Si

There total 8 articles about C₃₄H₅₆INO₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1378889-89-4
C₅₀H₇₄INO₇Si₂

: 1378889-91-8
C₃₄H₅₆INO₇Si

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃; for 6.08333h; Inert atmosphere;
DOI:10.1021/ol301103d

Reference yield:

: C₄₃H₆₆O₇Si₂

: 1378889-91-8
C₃₄H₅₆INO₇Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

1.2: 12 h / 20 °C / Inert atmosphere

2.1: sodium hydrogencarbonate; Dess-Martin periodane; tert-butyl alcohol / dichloromethane / 0.75 h / Inert atmosphere

3.1: 2,6-di-tert-butyl-4-methylpyridine; 1,2-dibromo-1,1,2,2-tetrachloroethane; triphenylphosphine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

3.2: 3 h / 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran; N,N-dimethyl-formamide / 6.08 h / 0 - 20 °C / Inert atmosphere

With 2,6-di-tert-butyl-4-methylpyridine; 1,2-dibromo-1,1,2,2-tetrachloroethane; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; triethylamine; triphenylphosphine; tert-butyl alcohol; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 2.1: Dess-Martin oxidation;
DOI:10.1021/ol301103d

Reference yield:

: C₅₀H₇₆INO₈Si₂

: 1378889-91-8
C₃₄H₅₆INO₇Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,6-di-tert-butyl-4-methylpyridine; 1,2-dibromo-1,1,2,2-tetrachloroethane; triphenylphosphine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

1.2: 3 h / 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran; N,N-dimethyl-formamide / 6.08 h / 0 - 20 °C / Inert atmosphere

With 2,6-di-tert-butyl-4-methylpyridine; 1,2-dibromo-1,1,2,2-tetrachloroethane; tetrabutyl ammonium fluoride; acetic acid; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol301103d