C₅₃H₇₀F₂N₄O₈Si₂

Base Information

Chemical Name:C₅₃H₇₀F₂N₄O₈Si₂
CAS No.:1343407-52-2
Molecular Formula:C₅₃H₇₀F₂N₄O₈Si₂
Molecular Weight:985.329
Hs Code.:

C<sub>53</sub>H<sub>70</sub>F<sub>2</sub>N<sub>4</sub>O<sub>8</sub>Si<sub>2</sub>

Synonyms:C₅₃H₇₀F₂N₄O₈Si₂

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Chemical Property of C₅₃H₇₀F₂N₄O₈Si₂

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Technology Process of C₅₃H₇₀F₂N₄O₈Si₂

There total 10 articles about C₅₃H₇₀F₂N₄O₈Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1343407-51-1
C₅₃H₆₆F₂N₄O₁₂Si₂

: 1343407-52-2
C₅₃H₇₀F₂N₄O₈Si₂

Guidance literature:: C₅₃H₆₆F₂N₄O₁₂Si₂; With formic acid; zinc; In ethanol; at 20 ℃; for 0.416667h;

With sodium hydrogencarbonate; In water; ethyl acetate;

Reference yield:

: 1201630-40-1
1,1‘-[[(propane-1,3-diyl)dioxy]bis[(5-methoxy-2-nitro-1,4-phenylene)carbonyl]]bis[(2S,4R)-methyl-4-hydroxypyrrolidine-2-carboxylate]

: 1343407-52-2
C₅₃H₇₀F₂N₄O₈Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: trichloroisocyanuric acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0.5 h / 0 °C

2: 2,6-dimethylpyridine / dichloromethane / 1 h / -45 - 40 °C / Inert atmosphere

3: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / Inert atmosphere

4: lithium borohydride; ethanol / ethanol; tetrahydrofuran / 1 h / 15 - 25 °C / Cooling with ice

5: 1H-imidazole / dichloromethane / 2 h / 0 - 20 °C

6: zinc; formic acid / ethanol / 0.42 h / 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; lithium borohydride; formic acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; ethanol; trichloroisocyanuric acid; sodium carbonate; zinc; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; dichloromethane; water; toluene; 3: Suzuki Coupling;

Reference yield:

: 1343407-47-5
C₃₁H₃₂N₄O₁₆

: 1343407-52-2
C₅₃H₇₀F₂N₄O₈Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: 2,6-dimethylpyridine / dichloromethane / 1 h / -45 - 40 °C / Inert atmosphere

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / Inert atmosphere

3: lithium borohydride; ethanol / ethanol; tetrahydrofuran / 1 h / 15 - 25 °C / Cooling with ice

4: 1H-imidazole / dichloromethane / 2 h / 0 - 20 °C

5: zinc; formic acid / ethanol / 0.42 h / 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; lithium borohydride; formic acid; ethanol; sodium carbonate; zinc; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; dichloromethane; water; toluene; 2: Suzuki Coupling;