Trifluoro-acetic acid 4-(tert-butyl-dimethyl-silanyloxy)-2,3,5,6-tetramethyl-phenyl ester

Base Information

• Chemical Name: Trifluoro-acetic acid 4-(tert-butyl-dimethyl-silanyloxy)-2,3,5,6-tetramethyl-phenyl ester
• CAS No.: 173069-11-9
• Molecular Formula: C₁₈H₂₇F₃O₃Si
• Molecular Weight: 376.491

Synonyms:Trifluoro-acetic acid 4-(tert-butyl-dimethyl-silanyloxy)-2,3,5,6-tetramethyl-phenyl ester

Chemical Property of Trifluoro-acetic acid 4-(tert-butyl-dimethyl-silanyloxy)-2,3,5,6-tetramethyl-phenyl ester

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Technology Process of Trifluoro-acetic acid 4-(tert-butyl-dimethyl-silanyloxy)-2,3,5,6-tetramethyl-phenyl ester

There total 19 articles about Trifluoro-acetic acid 4-(tert-butyl-dimethyl-silanyloxy)-2,3,5,6-tetramethyl-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

tert-Butyl-(4-methanesulfinyl-2,3,5,6-tetramethyl-phenoxy)-dimethyl-silane (173069-09-5) + trifluoroacetic anhydride (407-25-0) → tert-Butyl-dimethyl-(2,3,5,6-tetramethyl-4-methylsulfanyl-phenoxy)-silane + Trifluoro-acetic acid 4-(tert-butyl-dimethyl-silanyloxy)-2,3,5,6-tetramethyl-phenyl ester (173069-11-9) + Trifluoro-acetic acid 4-(tert-butyl-dimethyl-silanyloxy)-2,3,5,6-tetramethyl-phenylsulfanylmethyl ester

Guidance literature:

In chloroform; at 0 ℃; for 0.166667h;

DOI:10.1039/c39950002319

Reference yield: 79.0%

(4-Benzenesulfinyl-2,3,5,6-tetramethyl-phenoxy)-tert-butyl-dimethyl-silane (173069-06-2) + trifluoroacetic anhydride (407-25-0) → Trifluoro-acetic acid 4-(tert-butyl-dimethyl-silanyloxy)-2,3,5,6-tetramethyl-phenyl ester (173069-11-9)

Guidance literature:

With styrene; In chloroform; for 1h; 0 deg C to r.t.;

DOI:10.1039/c39950002319

Reference yield: 73.0%

tert-Butyl-[4-(4-methoxy-benzenesulfinyl)-2,3,5,6-tetramethyl-phenoxy]-dimethyl-silane (173069-07-3) + trifluoroacetic anhydride (407-25-0) → tert-Butyl-[4-(4-methoxy-phenylsulfanyl)-2,3,5,6-tetramethyl-phenoxy]-dimethyl-silane + Trifluoro-acetic acid 4-(tert-butyl-dimethyl-silanyloxy)-2,3,5,6-tetramethyl-phenyl ester (173069-11-9)

Guidance literature:

In chloroform; at 0 ℃; for 0.5h;

DOI:10.1021/jo970418o

upstream raw materials:

tert-Butyl-dimethyl-[2,3,5,6-tetramethyl-4-(2-methyl-propane-2-sulfinyl)-phenoxy]-silane

(4-Benzenesulfinyl-2,3,5,6-tetramethyl-phenoxy)-tert-butyl-dimethyl-silane

tert-Butyl-[4-(4-methoxy-benzenesulfinyl)-2,3,5,6-tetramethyl-phenoxy]-dimethyl-silane

tert-Butyl-(4-methanesulfinyl-2,3,5,6-tetramethyl-phenoxy)-dimethyl-silane

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