Technology Process of C24H29Cl2N5O2
There total 11 articles about C24H29Cl2N5O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
dichloromethane; ethyl acetate;
at 23 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: triethylamine; HATU / dichloromethane / 12 h / 0 - 20 °C
2.1: acetic acid / toluene / 0.5 h / 100 °C
3.1: acetic acid; zinc / dichloromethane / 1 h / 20 °C
4.1: acetic acid / water / 5 h / 23 °C
5.1: triethylamine; methanesulfonyl chloride / dichloromethane / 1 h / 0 - 20 °C
5.2: 2 h / 100 °C
6.1: lithium hydroxide monohydrate / water; tetrahydrofuran / 5 h / 23 °C
7.1: triethylamine; HATU; hydroxylamine hydrochloride / dichloromethane / 5 h / 20 °C
8.1: hydrogenchloride / dichloromethane; ethyl acetate / 2 h / 23 °C
With
hydrogenchloride; lithium hydroxide monohydrate; hydroxylamine hydrochloride; acetic acid; methanesulfonyl chloride; triethylamine; HATU; zinc;
In
tetrahydrofuran; dichloromethane; water; ethyl acetate; toluene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: acetic acid; zinc / dichloromethane / 1 h / 20 °C
2.1: acetic acid / water / 5 h / 23 °C
3.1: triethylamine; methanesulfonyl chloride / dichloromethane / 1 h / 0 - 20 °C
3.2: 2 h / 100 °C
4.1: lithium hydroxide monohydrate / water; tetrahydrofuran / 5 h / 23 °C
5.1: triethylamine; HATU; hydroxylamine hydrochloride / dichloromethane / 5 h / 20 °C
6.1: hydrogenchloride / dichloromethane; ethyl acetate / 2 h / 23 °C
With
hydrogenchloride; lithium hydroxide monohydrate; hydroxylamine hydrochloride; acetic acid; methanesulfonyl chloride; triethylamine; HATU; zinc;
In
tetrahydrofuran; dichloromethane; water; ethyl acetate;