C₂₃H₃₃N₃O₅S

Base Information

Chemical Name:C₂₃H₃₃N₃O₅S
CAS No.:143840-55-5
Molecular Formula:C₂₃H₃₃N₃O₅S
Molecular Weight:463.598
Hs Code.:

C<sub>23</sub>H<sub>33</sub>N<sub>3</sub>O<sub>5</sub>S

Synonyms:C₂₃H₃₃N₃O₅S

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Chemical Property of C₂₃H₃₃N₃O₅S

Chemical Property:

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Technology Process of C₂₃H₃₃N₃O₅S

There total 9 articles about C₂₃H₃₃N₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4289-98-9
N-formyl-L-methionine

: C₁₇H₂₄N₂O₃

: 143840-55-5
C₂₃H₃₃N₃O₅S

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 12h; Enzymatic reaction;
DOI:10.1016/j.bmc.2012.11.046

Reference yield:

: 123806-63-3,123039-88-3,197778-15-7
methyl (1R,2S)-1-amino-2-phenylcyclopropanecarboxylate

: 143840-55-5
C₂₃H₃₃N₃O₅S

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane; tetrahydrofuran / 5.25 h / -15 - 20 °C

2: trifluoroacetic acid / 0.5 h / Cooling with ice; Enzymatic reaction

3: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 0 - 20 °C / Enzymatic reaction

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.11.046

Reference yield:

: C₂₅H₂₂N₂O₆

: 143840-55-5
C₂₃H₃₃N₃O₅S

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydroxide / 1,4-dioxane; water / 4 h / 20 °C

2.1: brucine / water; ethanol / 20 °C

2.2: Dowex 50w

3.1: sulfuric acid / 48 h / 20 °C

4.1: trifluoroacetic acid; methyl-phenyl-thioether / 12 h / 20 °C

5.1: triethylamine / dichloromethane; tetrahydrofuran / 5.25 h / -15 - 20 °C

6.1: trifluoroacetic acid / 0.5 h / Cooling with ice; Enzymatic reaction

7.1: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 0 - 20 °C / Enzymatic reaction

With methyl-phenyl-thioether; sulfuric acid; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; brucine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.11.046