2-Benzyl-3,4-dihydro-4-methyl-5-phenyl-2H-1,2,6-thiadiazin-1,1,6-trioxid

Base Information

Chemical Name:2-Benzyl-3,4-dihydro-4-methyl-5-phenyl-2H-1,2,6-thiadiazin-1,1,6-trioxid
CAS No.:127446-11-1
Molecular Formula:C₁₇H₁₈N₂O₃S
Molecular Weight:330.408
Hs Code.:

Synonyms:2-Benzyl-3,4-dihydro-4-methyl-5-phenyl-2H-1,2,6-thiadiazin-1,1,6-trioxid

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Chemical Property of 2-Benzyl-3,4-dihydro-4-methyl-5-phenyl-2H-1,2,6-thiadiazin-1,1,6-trioxid

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Technology Process of 2-Benzyl-3,4-dihydro-4-methyl-5-phenyl-2H-1,2,6-thiadiazin-1,1,6-trioxid

There total 4 articles about 2-Benzyl-3,4-dihydro-4-methyl-5-phenyl-2H-1,2,6-thiadiazin-1,1,6-trioxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

: 127446-04-2
3-(Benzylamino)-2-methyl-1-phenyl-1-propanon-(Z)-oxim

: 127446-11-1
2-Benzyl-3,4-dihydro-4-methyl-5-phenyl-2H-1,2,6-thiadiazin-1,1,6-trioxid

Guidance literature:: With sulfuryl dichloride; triethylamine; In tetrahydrofuran; water; at 0 ℃;

Reference yield:

: 3287-99-8,39110-74-2,108321-65-9
benzylamine hydrochloride

: 127446-11-1
2-Benzyl-3,4-dihydro-4-methyl-5-phenyl-2H-1,2,6-thiadiazin-1,1,6-trioxid

Guidance literature:: Multi-step reaction with 3 steps

1: 41 percent / konz. HCl / aq. ethanol / 6 h / Heating

2: 56 percent / NH₂OH*HCl, NaOAc / methanol; H₂O / 40 °C

3: 7 percent / SO₂Cl₂, Et₃N / tetrahydrofuran; H₂O / 0 °C

With hydrogenchloride; sulfuryl dichloride; hydroxylamine hydrochloride; sodium acetate; triethylamine; In tetrahydrofuran; methanol; ethanol; water;

Reference yield:

: 127446-00-8
1-(Benzylamino)-2-methyl-1-phenyl-1-propanon-hydrochlorid

: 127446-11-1
2-Benzyl-3,4-dihydro-4-methyl-5-phenyl-2H-1,2,6-thiadiazin-1,1,6-trioxid

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / NH₂OH*HCl, NaOAc / methanol; H₂O / 40 °C

2: 7 percent / SO₂Cl₂, Et₃N / tetrahydrofuran; H₂O / 0 °C

With sulfuryl dichloride; hydroxylamine hydrochloride; sodium acetate; triethylamine; In tetrahydrofuran; methanol; water;