<1S,2R>-1-<<2-(benzoylthio)cyclopentyl>carbonyl>-L-proline 1,1-dimethylethyl ester

Base Information

Chemical Name:<1S,2R>-1-<<2-(benzoylthio)cyclopentyl>carbonyl>-L-proline 1,1-dimethylethyl ester
CAS No.:80969-61-5
Molecular Formula:C₂₂H₂₉NO₄S
Molecular Weight:403.543
Hs Code.:

Synonyms:<1S,2R>-1-<<2-(benzoylthio)cyclopentyl>carbonyl>-L-proline 1,1-dimethylethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <1S,2R>-1-<<2-(benzoylthio)cyclopentyl>carbonyl>-L-proline 1,1-dimethylethyl ester

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Technology Process of <1S,2R>-1-<<2-(benzoylthio)cyclopentyl>carbonyl>-L-proline 1,1-dimethylethyl ester

There total 5 articles about <1S,2R>-1-<<2-(benzoylthio)cyclopentyl>carbonyl>-L-proline 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.5%

: 2812-46-6
proline tert-butyl ester

: 99343-54-1
trans-2-(benzoylthio)cyclopentanecarboxylic acid

: 80969-61-5
<1S,2R>-1-<<2-(benzoylthio)cyclopentyl>carbonyl>-L-proline 1,1-dimethylethyl ester

: 81024-72-8
<1R,2S>-1-<<2-(benzoylthio)cyclopentyl>carbonyl>-L-proline 1,1-dimethylethyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 5 ℃; for 4h;
DOI:10.1021/jm00153a017

Reference yield:

: 98-91-9
thiobenzoic acid

: 80969-61-5
<1S,2R>-1-<<2-(benzoylthio)cyclopentyl>carbonyl>-L-proline 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 27.6 percent / 120 °C

2: 42.1 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / 4 h / 0 - 5 °C

With dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/jm00153a017

Reference yield:

: 1560-11-8
cyclopent-1-enecarboxylic acid

: 80969-61-5
<1S,2R>-1-<<2-(benzoylthio)cyclopentyl>carbonyl>-L-proline 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 27.6 percent / 120 °C

2: 42.1 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / 4 h / 0 - 5 °C

With dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/jm00153a017