5-(benzyloxy)-1-hydroxy-2,2-indandipropionic acid δ-lactone

Base Information

Chemical Name:5-(benzyloxy)-1-hydroxy-2,2-indandipropionic acid δ-lactone
CAS No.:90606-46-5
Molecular Formula:C₂₂H₂₂O₅
Molecular Weight:366.414
Hs Code.:

Synonyms:5-(benzyloxy)-1-hydroxy-2,2-indandipropionic acid δ-lactone

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Chemical Property of 5-(benzyloxy)-1-hydroxy-2,2-indandipropionic acid δ-lactone

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Technology Process of 5-(benzyloxy)-1-hydroxy-2,2-indandipropionic acid δ-lactone

There total 3 articles about 5-(benzyloxy)-1-hydroxy-2,2-indandipropionic acid δ-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 90606-45-4
5-(benzyloxy)-1-oxo-2,2-indandipropionic acid

: 90606-46-5
5-(benzyloxy)-1-hydroxy-2,2-indandipropionic acid δ-lactone

Guidance literature:: With sodium hydroxide; sodium tetrahydroborate; for 144h; Ambient temperature;
DOI:10.1021/jm00375a023

Reference yield:

: 78326-88-2
5-benzyloxy-1-indanone

: 90606-46-5
5-(benzyloxy)-1-hydroxy-2,2-indandipropionic acid δ-lactone

Guidance literature:: Multi-step reaction with 3 steps

1: t-BuOK / 2-methyl-propan-2-ol

2: 10percent aq. NaOH

3: 90 percent / NaBH₄, 0.2N aq. NaOH / 144 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; potassium tert-butylate; In tert-butyl alcohol;
DOI:10.1021/jm00375a023

Reference yield:

: 90606-44-3
dimethyl 5-benzyloxy-1-oxo-2,2-indandipropionate

: 90606-46-5
5-(benzyloxy)-1-hydroxy-2,2-indandipropionic acid δ-lactone

Guidance literature:: Multi-step reaction with 2 steps

1: 10percent aq. NaOH

2: 90 percent / NaBH₄, 0.2N aq. NaOH / 144 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate;
DOI:10.1021/jm00375a023