5,10,15-tris[(4'''-sulfuric acid)phenyl]-20-(1',1',3',3'-tetramethylisoindolin-2'-yloxyl-5'-yl)porphyrin

Base Information

• Chemical Name: 5,10,15-tris[(4'''-sulfuric acid)phenyl]-20-(1',1',3',3'-tetramethylisoindolin-2'-yloxyl-5'-yl)porphyrin
• CAS No.: 1370037-32-3
• Molecular Formula: C₅₀H₄₀N₅O₁₀S₃
• Molecular Weight: 967.093

Synonyms:5,10,15-tris[(4'''-sulfuric acid)phenyl]-20-(1',1',3',3'-tetramethylisoindolin-2'-yloxyl-5'-yl)porphyrin

Chemical Property of 5,10,15-tris[(4'''-sulfuric acid)phenyl]-20-(1',1',3',3'-tetramethylisoindolin-2'-yloxyl-5'-yl)porphyrin

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Technology Process of 5,10,15-tris[(4'''-sulfuric acid)phenyl]-20-(1',1',3',3'-tetramethylisoindolin-2'-yloxyl-5'-yl)porphyrin

There total 3 articles about 5,10,15-tris[(4'''-sulfuric acid)phenyl]-20-(1',1',3',3'-tetramethylisoindolin-2'-yloxyl-5'-yl)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

5,10,15-trisphenyl-20-(1',1',3',3'-tetramethylisoindolin-2'-yloxyl-5'-yl)porphyrin (1370037-27-6) → 5,10,15-tris[(4'''-sulfuric acid)phenyl]-20-(1',1',3',3'-tetramethylisoindolin-2'-yloxyl-5'-yl)porphyrin (1370037-32-3)

Guidance literature:

5,10,15-trisphenyl-20-(1',1',3',3'-tetramethylisoindolin-2'-yloxyl-5'-yl)porphyrin; With sulfuric acid; In water; at 20 - 70 ℃; for 168h; Inert atmosphere;

With sodium hydroxide; pH=10; Inert atmosphere;

DOI:10.1142/S1088424611003203

Reference yield:

5-phenyldipyrromethane (107798-98-1) → 5,10,15-tris[(4'''-sulfuric acid)phenyl]-20-(1',1',3',3'-tetramethylisoindolin-2'-yloxyl-5'-yl)porphyrin (1370037-32-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 1 h / 20 °C / Inert atmosphere; Darkness

1.2: 1 h / Inert atmosphere

2.1: sulfuric acid / water / 168 h / 20 - 70 °C / Inert atmosphere

2.2: pH 10 / Inert atmosphere

With sulfuric acid; boron trifluoride diethyl etherate; In dichloromethane; water;

DOI:10.1142/S1088424611003203

Reference yield:

5-formyl-1,1,3,3-tetramethylisoindolin-2-yloxyl (276885-27-9) → 5,10,15-tris[(4'''-sulfuric acid)phenyl]-20-(1',1',3',3'-tetramethylisoindolin-2'-yloxyl-5'-yl)porphyrin (1370037-32-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 1 h / 20 °C / Inert atmosphere; Darkness

1.2: 1 h / Inert atmosphere

2.1: sulfuric acid / water / 168 h / 20 - 70 °C / Inert atmosphere

2.2: pH 10 / Inert atmosphere

With sulfuric acid; boron trifluoride diethyl etherate; In dichloromethane; water;

DOI:10.1142/S1088424611003203

upstream raw materials:

5,10,15-trisphenyl-20-(1',1',3',3'-tetramethylisoindolin-2'-yloxyl-5'-yl)porphyrin

5-phenyldipyrromethane

5-formyl-1,1,3,3-tetramethylisoindolin-2-yloxyl

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