(1S,3S,5R)-3-Benzenesulfonyl-6-oxa-bicyclo[3.1.0]hexane-3-carboxylic acid benzyl ester

Base Information

Chemical Name:(1S,3S,5R)-3-Benzenesulfonyl-6-oxa-bicyclo[3.1.0]hexane-3-carboxylic acid benzyl ester
CAS No.:110745-59-0
Molecular Formula:C₁₉H₁₈O₅S
Molecular Weight:358.415
Hs Code.:

Synonyms:(1S,3S,5R)-3-Benzenesulfonyl-6-oxa-bicyclo[3.1.0]hexane-3-carboxylic acid benzyl ester

Suppliers and Price of (1S,3S,5R)-3-Benzenesulfonyl-6-oxa-bicyclo[3.1.0]hexane-3-carboxylic acid benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,3S,5R)-3-Benzenesulfonyl-6-oxa-bicyclo[3.1.0]hexane-3-carboxylic acid benzyl ester

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Technology Process of (1S,3S,5R)-3-Benzenesulfonyl-6-oxa-bicyclo[3.1.0]hexane-3-carboxylic acid benzyl ester

There total 1 articles about (1S,3S,5R)-3-Benzenesulfonyl-6-oxa-bicyclo[3.1.0]hexane-3-carboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 110745-58-9
1-Benzenesulfonyl-cyclopent-3-enecarboxylic acid benzyl ester

: 110745-59-0
(1S,3S,5R)-3-Benzenesulfonyl-6-oxa-bicyclo[3.1.0]hexane-3-carboxylic acid benzyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃;
DOI:10.1021/jo00232a051

Reference yield: 97.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 110745-59-0
(1S,3S,5R)-3-Benzenesulfonyl-6-oxa-bicyclo[3.1.0]hexane-3-carboxylic acid benzyl ester

: (1S,4S)-1-Benzenesulfonyl-4-(tert-butyl-dimethyl-silanyloxy)-cyclopent-2-enecarboxylic acid benzyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; In benzene; for 5h; Ambient temperature;
DOI:10.1021/jo00232a051

Reference yield:

: 110745-59-0
(1S,3S,5R)-3-Benzenesulfonyl-6-oxa-bicyclo[3.1.0]hexane-3-carboxylic acid benzyl ester

: 110850-51-6
1-Benzenesulfonyl-4-oxo-cyclopent-2-enecarboxylic acid (3Z,5E)-(1R,2R)-6-ethoxy-1,2-dimethyl-hexa-3,5-dienyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / diisopropylethylamine, DBU / benzene / 5 h / Ambient temperature

2: 90 percent / 10percent Pd/C / ethanol; various solvent(s)

With 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1021/jo00232a051