Technology Process of C25H22B2O7
There total 10 articles about C25H22B2O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridine
2: HCl; ZnCl2
3: LDA / tetrahydrofuran
4: PdCl2(dppf); KOAc / dimethylsulfoxide
5: TiCl3; LiAlH4
6: LiAlH4
With
pyridine; hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; lithium aluminium tetrahydride; titanium(III) chloride; potassium acetate; zinc(II) chloride; lithium diisopropyl amide;
In
tetrahydrofuran; dimethyl sulfoxide;
5: McMurry reaction;
DOI:10.1002/1521-3773(20010504)40:9<1714::AID-ANIE17140>3.0.CO;2-F
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: LDA
2.1: tosyl azide; Et3N
2.2: Rh(OAc)2
3.1: LDA / tetrahydrofuran
4.1: PdCl2(dppf); KOAc / dimethylsulfoxide
5.1: TiCl3; LiAlH4
6.1: LiAlH4
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; lithium aluminium tetrahydride; 4-toluenesulfonyl azide; titanium(III) chloride; potassium acetate; triethylamine; lithium diisopropyl amide;
In
tetrahydrofuran; dimethyl sulfoxide;
5.1: McMurry reaction;
DOI:10.1002/1521-3773(20010504)40:9<1714::AID-ANIE17140>3.0.CO;2-F
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: SmI3
2.1: LDA
3.1: tosyl azide; Et3N
3.2: Rh(OAc)2
4.1: LDA / tetrahydrofuran
5.1: PdCl2(dppf); KOAc / dimethylsulfoxide
6.1: TiCl3; LiAlH4
7.1: LiAlH4
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; lithium aluminium tetrahydride; 4-toluenesulfonyl azide; titanium(III) chloride; samarium (III) iodide; potassium acetate; triethylamine; lithium diisopropyl amide;
In
tetrahydrofuran; dimethyl sulfoxide;
6.1: McMurry reaction;
DOI:10.1002/1521-3773(20010504)40:9<1714::AID-ANIE17140>3.0.CO;2-F