C₃₉H₅₄O₄Sn

Base Information

• Chemical Name: C₃₉H₅₄O₄Sn
• CAS No.: 1092981-91-3
• Molecular Formula: C₃₉H₅₄O₄Sn
• Molecular Weight: 705.565

Synonyms:C₃₉H₅₄O₄Sn

Chemical Property of C₃₉H₅₄O₄Sn

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Technology Process of C₃₉H₅₄O₄Sn

There total 1 articles about C₃₉H₅₄O₄Sn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,5-anhydro-2-deoxy-3,4,6-O-tris-phenylmethyl-1-[(Ss)-phenylsulfinyl]-D-lyxo-hex-1-enitol + tributyltin chloride (1461-22-9) → C39H54O4Sn (1092981-91-3)

Guidance literature:

1,5-anhydro-2-deoxy-3,4,6-O-tris-phenylmethyl-1-[(Ss)-phenylsulfinyl]-D-lyxo-hex-1-enitol; With phenyllithium; Inert atmosphere;

tributyltin chloride; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

DOI:10.1080/07328303.2018.1508590

Reference yield: 84.0%

C39H54O4Sn (1092981-91-3) → 2,6:7,11-dianhydro-5,8-dideoxy-1,3,4,9,10,12-hexakis-O-benzyl-D-threo-L-galododeco-5,7-dienitol

Guidance literature:

With dichloro bis(acetonitrile) palladium(II); copper(I) thiophene-2-carboxylate; In N,N-dimethyl-formamide; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1080/07328303.2018.1508590

Reference yield: 56.0%

n-butyllithium (109-72-8,29786-93-4) + C39H54O4Sn (1092981-91-3) → (2R,3S,4R,E)-1,3,4-tris(benzyloxy)dec-5-en-2-ol (1374871-05-2)

Guidance literature:

n-butyllithium; With copper(l) cyanide; In diethyl ether; hexane; at -78 - 0 ℃; for 0.166667h; Inert atmosphere;

C₃₉H₅₄O₄Sn; In diethyl ether; hexane; at -35 - 0 ℃; for 2.5h; Inert atmosphere;

DOI:10.1055/s-0031-1289721

upstream raw materials:

tributyltin chloride

Downstream raw materials:

(2R,3S,4R,E)-1,3,4-tris(benzyloxy)dec-5-en-2-ol

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