phenylbis(thiophen-2-yl)methanol

Base Information

• Chemical Name: phenylbis(thiophen-2-yl)methanol
• CAS No.: 92724-31-7
• Molecular Formula: C₁₅H₁₂OS₂
• Molecular Weight: 272.392
• Mol file: 92724-31-7.mol

Synonyms:phenylbis(thiophen-2-yl)methanol

Chemical Property of phenylbis(thiophen-2-yl)methanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of phenylbis(thiophen-2-yl)methanol

There total 3 articles about phenylbis(thiophen-2-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-thienyl lithium (2786-07-4) + benzoic acid methyl ester (93-58-3,5705-52-2,80226-58-0) → phenylbis(thiophen-2-yl)methanol (92724-31-7)

Guidance literature:

In tetrahydrofuran; hexane; water; at 25 ℃; for 0.00555556h; Solvent;

DOI:10.1016/j.tet.2020.131898

Reference yield:

2-thienylmagnesium iodide (89180-57-4) → phenylbis(thiophen-2-yl)methanol (92724-31-7)

Guidance literature:

Reference yield:

→ phenylbis(thiophen-2-yl)methanol (92724-31-7)

Guidance literature:

Benzoesaeure-ethylester in Bzl., 1) Eintragen in ether. Lsg. v. Thiophenyl-(2)-MgBr, 2) Erwaermen;

DOI:10.1039/jr9620003235

upstream raw materials:

2-thienyl lithium

benzoic acid methyl ester

2-thienylmagnesium iodide

Downstream raw materials:

C₁₅H₁₁S₂⁽¹⁺⁾