3-(4-(3-(4-(3-(7,8-dimethoxy-1-m-tolyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)propyl)-1H-1,2,3-triazol-1-yl)propyl)piperazin-1-yl)benzo[d]isothiazole

Base Information

Chemical Name:3-(4-(3-(4-(3-(7,8-dimethoxy-1-m-tolyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)propyl)-1H-1,2,3-triazol-1-yl)propyl)piperazin-1-yl)benzo[d]isothiazole
CAS No.:1186236-41-8
Molecular Formula:C₃₈H₄₇N₇O₂S
Molecular Weight:665.903
Hs Code.:

Synonyms:3-(4-(3-(4-(3-(7,8-dimethoxy-1-m-tolyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)propyl)-1H-1,2,3-triazol-1-yl)propyl)piperazin-1-yl)benzo[d]isothiazole

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Chemical Property of 3-(4-(3-(4-(3-(7,8-dimethoxy-1-m-tolyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)propyl)-1H-1,2,3-triazol-1-yl)propyl)piperazin-1-yl)benzo[d]isothiazole

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Technology Process of 3-(4-(3-(4-(3-(7,8-dimethoxy-1-m-tolyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)propyl)-1H-1,2,3-triazol-1-yl)propyl)piperazin-1-yl)benzo[d]isothiazole

There total 1 articles about 3-(4-(3-(4-(3-(7,8-dimethoxy-1-m-tolyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)propyl)-1H-1,2,3-triazol-1-yl)propyl)piperazin-1-yl)benzo[d]isothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1186236-59-8
3-(4-(3-azidopropyl)piperazin-1-yl)benzo[d]isothiazole

: 1186236-34-9
7,8-dimethoxy-3-(pent-4-ynyl)-1-m-tolyl-2,3,4,5-tetrahydro-1H-benzo[d]azepine

: 1186236-41-8
3-(4-(3-(4-(3-(7,8-dimethoxy-1-m-tolyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)propyl)-1H-1,2,3-triazol-1-yl)propyl)piperazin-1-yl)benzo[d]isothiazole

Guidance literature:: With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.bmc.2009.06.019

Reference yield: 28.0%

: 1186236-41-8
3-(4-(3-(4-(3-(7,8-dimethoxy-1-m-tolyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)propyl)-1H-1,2,3-triazol-1-yl)propyl)piperazin-1-yl)benzo[d]isothiazole

: 3-(3-(1-(3-(4-(benzo[d]isothiazol-3-yl)piperazin-1-yl)-propyl)-1H-1,2,3-triazol-4-yl)propyl)-1-m-tolyl-2,3,4,5-tetrahydro-1H-benzo[d]azepine-7,8-diol 1.3-hydrobromide

Guidance literature:: 3-(4-(3-(4-(3-(7,8-dimethoxy-1-m-tolyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)propyl)-1H-1,2,3-triazol-1-yl)propyl)piperazin-1-yl)benzo[d]isothiazole; With boron tribromide; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;

With methanol; In dichloromethane; at -78 ℃;
DOI:10.1016/j.bmc.2009.06.019