C₆₂H₁₀₀O₁₀Si₃

Base Information

Chemical Name:C₆₂H₁₀₀O₁₀Si₃
CAS No.:440643-03-8
Molecular Formula:C₆₂H₁₀₀O₁₀Si₃
Molecular Weight:1089.73
Hs Code.:

C<sub>62</sub>H<sub>100</sub>O<sub>10</sub>Si<sub>3</sub>

Synonyms:C₆₂H₁₀₀O₁₀Si₃

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Chemical Property of C₆₂H₁₀₀O₁₀Si₃

Chemical Property:

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Technology Process of C₆₂H₁₀₀O₁₀Si₃

There total 19 articles about C₆₂H₁₀₀O₁₀Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 440643-03-8
C₆₂H₁₀₀O₁₀Si₃

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / pyridine; DMAP / 15 h

2: aq. LiOH / tetrahydrofuran; 2-methyl-propan-2-ol / 2 h / 20 °C

3: 34.2 mg / benzene; methanol; hexane / 0.25 h / 20 °C

4: 91 percent / BF₃*Et₂O / diethyl ether / 0.5 h / -78 °C

With pyridine; dmap; lithium hydroxide; boron trifluoride diethyl etherate; In tetrahydrofuran; methanol; diethyl ether; hexane; tert-butyl alcohol; benzene;
DOI:10.1016/S0040-4020(02)00050-9

Reference yield:

: 214483-92-8
(3S,4E)-3-methyl-7-benzyloxy-4-heptenoic acid ethyl ester

: 440643-03-8
C₆₂H₁₀₀O₁₀Si₃

Guidance literature:: Multi-step reaction with 17 steps

1.1: 84 percent / HMDS; TMEDA; n-BuLi / tetrahydrofuran / 0 °C

2.1: 96 percent / aq. LiCl / dimethylsulfoxide / 0.67 h / 190 °C

3.1: AD-mix-α / 2-methyl-propan-2-ol; H2O / 24 h / 0 °C

4.1: CSA / benzene; methanol / 32 h

4.2: H₂ / Pd(OH)2 / ethanol / 12 h / 20 °C / 760 Torr

5.1: 98 percent / TFA / methanol / 0.83 h / Heating

6.1: 75 percent / NMO; 4 Angstroem molecular sieves; TPAP / 2-methyl-propan-2-ol; acetonitrile / 20 °C

7.1: pyridine / tetrahydrofuran; toluene / 0.75 h / -78 - 20 °C

7.2: 9-BBN / tetrahydrofuran; toluene / 0.5 h / 20 °C

7.3: 40 percent / NaBO₃*4H₂O / tetrahydrofuran; toluene / 2 h

8.1: Dess-Martin periodinane reagent / CH₂Cl₂ / 2.5 h / 20 °C

9.1: 77 percent / TiCl₄ / CH₂Cl₂ / 0.33 h / -78 °C

10.1: 91 percent / pyridine; DMAP / 27 h / 20 °C

11.1: 99 percent / IBr / toluene; CH₂Cl₂ / 3 h / -80 °C

12.1: 90 percent / aq. LiOH / 1,2-dimethoxy-ethane / 13 h / 60 °C

13.1: 90 percent / pyridine; DMAP / CH₂Cl₂ / 16 h / 20 °C

14.1: 99 percent / pyridine; DMAP / 15 h

15.1: aq. LiOH / tetrahydrofuran; 2-methyl-propan-2-ol / 2 h / 20 °C

16.1: 34.2 mg / benzene; methanol; hexane / 0.25 h / 20 °C

17.1: 91 percent / BF₃*Et₂O / diethyl ether / 0.5 h / -78 °C

With pyridine; dmap; lithium hydroxide; AD-mix-α; n-butyllithium; N-methyl-2-indolinone; tetrapropylammonium perruthennate; N,N,N,N,-tetramethylethylenediamine; 4 A molecular sieve; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; iodine(I) bromide; titanium tetrachloride; Dess-Martin periodane; 1,1,1,3,3,3-hexamethyl-disilazane; trifluoroacetic acid; lithium chloride; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; hexane; dichloromethane; water; dimethyl sulfoxide; toluene; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1016/S0040-4020(02)00050-9

Reference yield:

: 214483-93-9
(3E,5S,9S,10E)-5,9-dimethyl-1,13-bis(benzyloxy)-3,10-tridecadien-7-one

: 440643-03-8
C₆₂H₁₀₀O₁₀Si₃

Guidance literature:: Multi-step reaction with 15 steps

1.1: AD-mix-α / 2-methyl-propan-2-ol; H2O / 24 h / 0 °C

2.1: CSA / benzene; methanol / 32 h

2.2: H₂ / Pd(OH)2 / ethanol / 12 h / 20 °C / 760 Torr

3.1: 98 percent / TFA / methanol / 0.83 h / Heating

4.1: 75 percent / NMO; 4 Angstroem molecular sieves; TPAP / 2-methyl-propan-2-ol; acetonitrile / 20 °C

5.1: pyridine / tetrahydrofuran; toluene / 0.75 h / -78 - 20 °C

5.2: 9-BBN / tetrahydrofuran; toluene / 0.5 h / 20 °C

5.3: 40 percent / NaBO₃*4H₂O / tetrahydrofuran; toluene / 2 h

6.1: Dess-Martin periodinane reagent / CH₂Cl₂ / 2.5 h / 20 °C

7.1: 77 percent / TiCl₄ / CH₂Cl₂ / 0.33 h / -78 °C

8.1: 91 percent / pyridine; DMAP / 27 h / 20 °C

9.1: 99 percent / IBr / toluene; CH₂Cl₂ / 3 h / -80 °C

10.1: 90 percent / aq. LiOH / 1,2-dimethoxy-ethane / 13 h / 60 °C

11.1: 90 percent / pyridine; DMAP / CH₂Cl₂ / 16 h / 20 °C

12.1: 99 percent / pyridine; DMAP / 15 h

13.1: aq. LiOH / tetrahydrofuran; 2-methyl-propan-2-ol / 2 h / 20 °C

14.1: 34.2 mg / benzene; methanol; hexane / 0.25 h / 20 °C

15.1: 91 percent / BF₃*Et₂O / diethyl ether / 0.5 h / -78 °C

With pyridine; dmap; lithium hydroxide; AD-mix-α; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; iodine(I) bromide; titanium tetrachloride; Dess-Martin periodane; trifluoroacetic acid; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; hexane; dichloromethane; water; toluene; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1016/S0040-4020(02)00050-9