ethyl 2-(3-(2-methylquinolin-6-yl)propanamido)cyclohex-1-enecarboxylate

Base Information

Chemical Name:ethyl 2-(3-(2-methylquinolin-6-yl)propanamido)cyclohex-1-enecarboxylate
CAS No.:1616119-40-4
Molecular Formula:C₂₂H₂₆N₂O₃
Molecular Weight:366.46
Hs Code.:

Synonyms:ethyl 2-(3-(2-methylquinolin-6-yl)propanamido)cyclohex-1-enecarboxylate

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Chemical Property of ethyl 2-(3-(2-methylquinolin-6-yl)propanamido)cyclohex-1-enecarboxylate

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Technology Process of ethyl 2-(3-(2-methylquinolin-6-yl)propanamido)cyclohex-1-enecarboxylate

There total 5 articles about ethyl 2-(3-(2-methylquinolin-6-yl)propanamido)cyclohex-1-enecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1616119-33-5
(E)-ethyl 2-(3-(2-methylquinolin-6-yl)acrylamido)cyclohex-1-enecarboxylate

: 1616119-40-4
ethyl 2-(3-(2-methylquinolin-6-yl)propanamido)cyclohex-1-enecarboxylate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmc.2014.05.011

Reference yield:

: 1616119-20-0
ethyl 2-(2-bromoacetamido)cyclohex-1-enecarboxylate

: 1616119-40-4
ethyl 2-(3-(2-methylquinolin-6-yl)propanamido)cyclohex-1-enecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 3 h / Reflux

2: potassium tert-butylate / dimethyl sulfoxide / 2 h / 20 °C

3: hydrogen; palladium 10% on activated carbon / methanol; tetrahydrofuran

With palladium 10% on activated carbon; potassium tert-butylate; hydrogen; In tetrahydrofuran; methanol; dimethyl sulfoxide; benzene; 2: |Wittig Olefination;
DOI:10.1016/j.bmc.2014.05.011

Reference yield:

: 1616119-21-1
(2-((2-(ethoxycarbonyl)cyclohex-1-en-1-yl)amino)-2-oxoethyl)triphenylphosphonium bromide

: 1616119-40-4
ethyl 2-(3-(2-methylquinolin-6-yl)propanamido)cyclohex-1-enecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / dimethyl sulfoxide / 2 h / 20 °C

2: hydrogen; palladium 10% on activated carbon / methanol; tetrahydrofuran

With palladium 10% on activated carbon; potassium tert-butylate; hydrogen; In tetrahydrofuran; methanol; dimethyl sulfoxide; 1: |Wittig Olefination;
DOI:10.1016/j.bmc.2014.05.011