3-benzyl-1,1-(ethylenedioxy)-2-oxa-3-azonia-1-borata-1,2-dihydronaphthaline

Base Information

• Chemical Name: 3-benzyl-1,1-(ethylenedioxy)-2-oxa-3-azonia-1-borata-1,2-dihydronaphthaline
• CAS No.: 86744-06-1
• Molecular Formula: C₁₆H₁₆BNO₃
• Molecular Weight: 281.119

Synonyms:3-benzyl-1,1-(ethylenedioxy)-2-oxa-3-azonia-1-borata-1,2-dihydronaphthaline

Chemical Property of 3-benzyl-1,1-(ethylenedioxy)-2-oxa-3-azonia-1-borata-1,2-dihydronaphthaline

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Technology Process of 3-benzyl-1,1-(ethylenedioxy)-2-oxa-3-azonia-1-borata-1,2-dihydronaphthaline

There total 1 articles about 3-benzyl-1,1-(ethylenedioxy)-2-oxa-3-azonia-1-borata-1,2-dihydronaphthaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

C7H5BO2NCH2C6H5*0.2H2O → 3-benzyl-1,1-(ethylenedioxy)-2-oxa-3-azonia-1-borata-1,2-dihydronaphthaline (86744-06-1)

Guidance literature:

With ethylene glycol; In benzene; byproducts: water; equimol. quantities of the nitrone and HOCH2CH2OH were heated under reflux in benzene with water removal for 30 min; mixt. was cooled, ether added, ppt. was sepd. and recrystd. from THF-petroleum ether; elem. anal.;

DOI:10.1016/0022-328X(83)85166-3

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