Benzoic acid (E)-6-(2,2-dimethyl-6-methylene-cyclohexyl)-4-methyl-2-oxo-hex-3-enyl ester

Base Information

Chemical Name:Benzoic acid (E)-6-(2,2-dimethyl-6-methylene-cyclohexyl)-4-methyl-2-oxo-hex-3-enyl ester
CAS No.:183549-45-3
Molecular Formula:C₂₃H₃₀O₃
Molecular Weight:354.489
Hs Code.:

Synonyms:Benzoic acid (E)-6-(2,2-dimethyl-6-methylene-cyclohexyl)-4-methyl-2-oxo-hex-3-enyl ester

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Chemical Property of Benzoic acid (E)-6-(2,2-dimethyl-6-methylene-cyclohexyl)-4-methyl-2-oxo-hex-3-enyl ester

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Technology Process of Benzoic acid (E)-6-(2,2-dimethyl-6-methylene-cyclohexyl)-4-methyl-2-oxo-hex-3-enyl ester

There total 10 articles about Benzoic acid (E)-6-(2,2-dimethyl-6-methylene-cyclohexyl)-4-methyl-2-oxo-hex-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13720-12-2
4-(2',2'-Dimethyl-6'-methylidenecyclohexyl)butan-2-one

: 183549-45-3
Benzoic acid (E)-6-(2,2-dimethyl-6-methylene-cyclohexyl)-4-methyl-2-oxo-hex-3-enyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent

2: 94 percent / Red-Al, H⁺ / H₂O

3: 97 percent / Bu₄NF, DMAP

4: PCC

With dmap; tetrabutyl ammonium fluoride; hydrogen cation; sodium bis(2-methoxyethoxy)aluminium dihydride; pyridinium chlorochromate; In water;
DOI:10.1021/jo9610568

Reference yield:

: 13720-13-3
4-(6',6'-dimethyl-2'-methylenecyclohexyl)butan-2-ol

: 183549-45-3
Benzoic acid (E)-6-(2,2-dimethyl-6-methylene-cyclohexyl)-4-methyl-2-oxo-hex-3-enyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / DMSO, ClCOCOCl, Et₃N

2: 100 percent

3: 94 percent / Red-Al, H⁺ / H₂O

4: 97 percent / Bu₄NF, DMAP

5: PCC

With dmap; oxalyl dichloride; tetrabutyl ammonium fluoride; hydrogen cation; dimethyl sulfoxide; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; pyridinium chlorochromate; In water;
DOI:10.1021/jo9610568

Reference yield:

: 35319-19-8
3-(2,2-dimethyl-6-oxo-cyclohexyl)-propionic acid ethyl ester

: 183549-45-3
Benzoic acid (E)-6-(2,2-dimethyl-6-methylene-cyclohexyl)-4-methyl-2-oxo-hex-3-enyl ester

Guidance literature:: Multi-step reaction with 9 steps

1: 71 percent / TiCl₄, Zn

2: 98 percent / LiAlH₄

3: 96 percent / DMSO, ClCOCOCl, Et₃N

4: 100 percent

5: 98 percent / DMSO, ClCOCOCl, Et₃N

6: 100 percent

7: 94 percent / Red-Al, H⁺ / H₂O

8: 97 percent / Bu₄NF, DMAP

9: PCC

With dmap; lithium aluminium tetrahydride; oxalyl dichloride; tetrabutyl ammonium fluoride; hydrogen cation; titanium tetrachloride; dimethyl sulfoxide; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; pyridinium chlorochromate; zinc; In water;
DOI:10.1021/jo9610568