C₂₈H₂₄F₃NO₃SSe

Base Information

Chemical Name:C₂₈H₂₄F₃NO₃SSe
CAS No.:1332496-32-8
Molecular Formula:C₂₈H₂₄F₃NO₃SSe
Molecular Weight:590.525
Hs Code.:

C<sub>28</sub>H<sub>24</sub>F<sub>3</sub>NO<sub>3</sub>SSe

Synonyms:C₂₈H₂₄F₃NO₃SSe

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Chemical Property of C₂₈H₂₄F₃NO₃SSe

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Technology Process of C₂₈H₂₄F₃NO₃SSe

There total 11 articles about C₂₈H₂₄F₃NO₃SSe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1332495-43-8
C₃₀H₂₈F₃NO₃SSe

: 1332496-32-8
C₂₈H₂₄F₃NO₃SSe

Guidance literature:: C₃₀H₂₈F₃NO₃SSe; With water; lithium hydroxide; In tetrahydrofuran; at 0 ℃; for 1h;

With sodium hydrogen sulfate; In tetrahydrofuran;

Reference yield:

: 1332498-00-6
C₁₂H₁₀F₃NOSe

: 1332496-32-8
C₂₈H₂₄F₃NO₃SSe

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-chloro-succinimide; triphenylphosphine / dichloromethane / 1 h / 20 °C

2.1: isopropylmagnesium chloride / tetrahydrofuran / 0.17 h / 0 °C

2.2: 0.17 h / -78 °C

3.1: isopropylmagnesium chloride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

3.2: -78 - 20 °C

4.1: potassium carbonate / water; acetone / 4 h / 20 °C

5.1: water; lithium hydroxide / tetrahydrofuran / 1 h / 0 °C

With N-chloro-succinimide; water; isopropylmagnesium chloride; potassium carbonate; triphenylphosphine; lithium hydroxide; In tetrahydrofuran; dichloromethane; water; acetone;

Reference yield:

: 455-18-5
4-CF₃C₆H₄CN

: 1332496-32-8
C₂₈H₂₄F₃NO₃SSe

Guidance literature:: Multi-step reaction with 10 steps

1.1: hydrogenchloride; pyridine / ethanol / 2 h / Inert atmosphere; Reflux

2.1: tetrahydrofuran / 12.83 h / 20 - 80 °C / Reflux

2.2: 0.33 h / 20 °C

3.1: diisobutylaluminium hydride / dichloromethane; hexane / 1.5 h / -78 - -10 °C / Inert atmosphere

4.1: N-chloro-succinimide; triphenylphosphine / dichloromethane / 1 h / 20 °C

5.1: isopropylmagnesium chloride / tetrahydrofuran / 0.17 h / 0 °C

5.2: 0.17 h / -78 °C

6.1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / 20 °C

7.1: lithium diisopropyl amide / tetrahydrofuran / -78 - 20 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

9.1: potassium carbonate / water; acetone / 4 h / 20 °C

10.1: water; lithium hydroxide / tetrahydrofuran / 1 h / 0 °C

With pyridine; 1H-imidazole; hydrogenchloride; N-chloro-succinimide; tetrabutyl ammonium fluoride; water; isopropylmagnesium chloride; diisobutylaluminium hydride; potassium carbonate; triphenylphosphine; lithium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone;