2,4-Diphenylarsenin

Base Information

• Chemical Name: 2,4-Diphenylarsenin
• CAS No.: 63466-40-0
• Molecular Formula: C₁₇H₁₃As
• Molecular Weight: 292.212
• Mol file: 63466-40-0.mol

Synonyms:2,4-Diphenylarsenin

Chemical Property of 2,4-Diphenylarsenin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-Diphenylarsenin

There total 3 articles about 2,4-Diphenylarsenin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1,4-Dihydro-methoxy-1,4-diphenylarsenin (63428-62-6,65683-83-2,65683-84-3) → 2,4-Diphenylarsenin (63466-40-0)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; for 3h; Heating;

Reference yield: 61.0%

1,4-Diphenyl-1,4-dihydro-arsinin-4-ol (88257-66-3,88257-77-6) → 2,4-Diphenylarsenin (63466-40-0)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; for 2h; Heating;

DOI:10.1016/S0040-4039(00)88266-0

Reference yield:

phenyllithium (591-51-5) → 2,4-Diphenylarsenin (63466-40-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 37 percent / diethyl ether / -30 °C

2: 61 percent / pTosOH / benzene / 2 h / Heating

With toluene-4-sulfonic acid; In diethyl ether; benzene;

DOI:10.1016/S0040-4039(00)88266-0

upstream raw materials:

1,4-Dihydro-methoxy-1,4-diphenylarsenin

1,4-Diphenyl-1,4-dihydro-arsinin-4-ol

phenyllithium

Downstream raw materials:

Mo(CO)3AsC₅H₃C₆H₅C₆H₅