ethyl 2,3,4-trimethoxymandelate

Base Information

Chemical Name:ethyl 2,3,4-trimethoxymandelate
CAS No.:911047-43-3
Molecular Formula:C₁₃H₁₈O₆
Molecular Weight:270.282
Hs Code.:

Synonyms:ethyl 2,3,4-trimethoxymandelate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 2,3,4-trimethoxymandelate

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Technology Process of ethyl 2,3,4-trimethoxymandelate

There total 2 articles about ethyl 2,3,4-trimethoxymandelate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 107416-80-8
2,3,4-trimethoxyphenylglyoxylic acid ethyl ester

: 911047-43-3
ethyl 2,3,4-trimethoxymandelate

Guidance literature:: With sodium tetrahydroborate; In ethanol; at -30 ℃; for 0.25h;
DOI:10.1055/s-2006-942404

Reference yield:

: 634-36-6
1,2,3-trimethoxybenzene

: 911047-43-3
ethyl 2,3,4-trimethoxymandelate

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / AlCl₃ / CH₂Cl₂ / 1 h / 20 °C

2: 95 percent / NaBH₄ / ethanol / 0.25 h / -30 °C

With sodium tetrahydroborate; aluminium trichloride; In ethanol; dichloromethane; 1: Friedel-Crafts acylation;
DOI:10.1055/s-2006-942404