allyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-2-<(R)-3-dodecanoyloxytetradecanoylamino>-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranosyl>-α-D-glucopyranoside 4'-(diphenyl phosphate)

Base Information

• Chemical Name: allyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-2-<(R)-3-dodecanoyloxytetradecanoylamino>-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranosyl>-α-D-glucopyranoside 4'-(diphenyl phosphate)
• CAS No.: 98917-56-7
• Molecular Formula: C₁₂₃H₂₀₁N₂O₂₂P
• Molecular Weight: 2090.92

Synonyms:allyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-2-<(R)-3-dodecanoyloxytetradecanoylamino>-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranosyl>-α-D-glucopyranoside 4'-(diphenyl phosphate)

Chemical Property of allyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-2-<(R)-3-dodecanoyloxytetradecanoylamino>-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranosyl>-α-D-glucopyranoside 4'-(diphenyl phosphate)

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Technology Process of allyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-2-<(R)-3-dodecanoyloxytetradecanoylamino>-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranosyl>-α-D-glucopyranoside 4'-(diphenyl phosphate)

There total 3 articles about allyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-2-<(R)-3-dodecanoyloxytetradecanoylamino>-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranosyl>-α-D-glucopyranoside 4'-(diphenyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C26H50O4 (107856-74-6) + C97H153N2O19P → allyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-2-<(R)-3-dodecanoyloxytetradecanoylamino>-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranosyl>-α-D-glucopyranoside 4'-(diphenyl phosphate) (98917-56-7)

Guidance literature:

With dicyclohexyl-carbodiimide; In chloroform; for 17h; Yield given; Ambient temperature;

DOI:10.1246/bcsj.60.2205

Reference yield:

C26H50O4 (107856-74-6) + allyl 6-O-{2-deoxy-2-trichloroethoxycarbonylamino-3-O-[(R)-3-tetradecanoyloxytetradecanoyl]-4-O-diphenylphosphono-6-O-trichloroethoxycarbonyl-β-D-glucopyranosyl}-2-deoxy-2-[(R)-3-benzyloxytetradecanoylamino]-3-O-[(R)-3-benzyloxytetradecanoyl]-α-D-glucopyranoside (95991-03-0) → allyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-2-<(R)-3-dodecanoyloxytetradecanoylamino>-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-β-D-glucopyranosyl>-α-D-glucopyranoside 4'-(diphenyl phosphate) (98917-56-7)

Guidance literature:

With acetic acid; dicyclohexyl-carbodiimide; zinc; Yield given. Multistep reaction; 2.) CHCl₃, 17h, r.t.;

DOI:10.1016/S0040-4039(00)98548-4

Reference yield:

→ allyl 6-O-{2-deoxy-2-[(R)-3-dodecanoyloxytetradecanoylamino]-3-O-[(R)-3-tetradecanoyloxytetradecanoyl]-4-O-diphenylphosphono-β-D-glucopyranosyl}-2-deoxy-2-[(R)-3-benzyloxytetradecanoylamino]-3-O-[(R)-3-benzyloxytetradecanoyl]-α-D-glucopyranoside (98917-56-7)

Guidance literature:

upstream raw materials:

C₂₆H₅₀O₄

allyl 6-O-{2-deoxy-2-trichloroethoxycarbonylamino-3-O-[(R)-3-tetradecanoyloxytetradecanoyl]-4-O-diphenylphosphono-6-O-trichloroethoxycarbonyl-β-D-glucopyranosyl}-2-deoxy-2-[(R)-3-benzyloxytetradecanoylamino]-3-O-[(R)-3-benzyloxytetradecanoyl]-α-D-glucopyranoside

Downstream raw materials:

C₁₃₁H₂₀₉N₂O₂₃P

C₁₄₄H₂₂₇N₂O₂₉P

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