3-butyryl-4-<(2,6-dimethylphenyl)amino>-8-<3-(1-tritylimidazol-4-yl)propoxy>quinoline

Base Information

Chemical Name:3-butyryl-4-<(2,6-dimethylphenyl)amino>-8-<3-(1-tritylimidazol-4-yl)propoxy>quinoline
CAS No.:1026056-80-3
Molecular Formula:C₄₆H₄₄N₄O₂
Molecular Weight:684.881
Hs Code.:

Synonyms:3-butyryl-4-<(2,6-dimethylphenyl)amino>-8-<3-(1-tritylimidazol-4-yl)propoxy>quinoline

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Chemical Property of 3-butyryl-4-<(2,6-dimethylphenyl)amino>-8-<3-(1-tritylimidazol-4-yl)propoxy>quinoline

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Technology Process of 3-butyryl-4-<(2,6-dimethylphenyl)amino>-8-<3-(1-tritylimidazol-4-yl)propoxy>quinoline

There total 8 articles about 3-butyryl-4-<(2,6-dimethylphenyl)amino>-8-<3-(1-tritylimidazol-4-yl)propoxy>quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1-trityl-4-(3-bromopropyl)imidazole

: 164861-26-1
1-[4-(2,6-Dimethyl-phenylamino)-8-hydroxy-quinolin-3-yl]-butan-1-one

: 1026056-80-3
3-butyryl-4-<(2,6-dimethylphenyl)amino>-8-<3-(1-tritylimidazol-4-yl)propoxy>quinoline

Guidance literature:: With potassium carbonate; In butanone; for 17h; Heating;
DOI:10.1021/jm00014a026

Reference yield:

: 90-04-0
2-methoxy-phenylamine

: 1026056-80-3
3-butyryl-4-<(2,6-dimethylphenyl)amino>-8-<3-(1-tritylimidazol-4-yl)propoxy>quinoline

Guidance literature:: Multi-step reaction with 6 steps

1: 64 percent / 5 h

2: 63 percent / diphenyl ether / 1.5 h / Heating

3: POCl₃ / 0.5 h / Heating

4: BBr₃ / CH₂Cl₂ / -10 °C

5: dioxane / 2 h / Heating

6: 31 percent / K₂CO₃ / butan-2-one / 17 h / Heating

With boron tribromide; potassium carbonate; trichlorophosphate; In 1,4-dioxane; diphenylether; dichloromethane; butanone;
DOI:10.1021/jm00014a026

Reference yield:

: 3249-68-1
ethyl butyroyl acetate

: 1026056-80-3
3-butyryl-4-<(2,6-dimethylphenyl)amino>-8-<3-(1-tritylimidazol-4-yl)propoxy>quinoline

Guidance literature:: Multi-step reaction with 7 steps

1: Ac₂O

2: 64 percent / 5 h

3: 63 percent / diphenyl ether / 1.5 h / Heating

4: POCl₃ / 0.5 h / Heating

5: BBr₃ / CH₂Cl₂ / -10 °C

6: dioxane / 2 h / Heating

7: 31 percent / K₂CO₃ / butan-2-one / 17 h / Heating

With acetic anhydride; boron tribromide; potassium carbonate; trichlorophosphate; In 1,4-dioxane; diphenylether; dichloromethane; butanone;
DOI:10.1021/jm00014a026