C₁₅H₂₀O₄

Base Information

Chemical Name:C₁₅H₂₀O₄
CAS No.:1195988-16-9
Molecular Formula:C₁₅H₂₀O₄
Molecular Weight:264.321
Hs Code.:

C<sub>15</sub>H<sub>20</sub>O<sub>4</sub>

Synonyms:C₁₅H₂₀O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₀O₄

Chemical Property:

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Technology Process of C₁₅H₂₀O₄

There total 4 articles about C₁₅H₂₀O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1195988-15-8
C₁₅H₂₀O₃

: 1195988-16-9
C₁₅H₂₀O₄

Guidance literature:: C₁₅H₂₀O₃; With titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; Cumene hydroperoxide; In dichloromethane; at -40 - -25 ℃; for 9h; Molecular sieve;

With tributylphosphine; citric acid; In dichloromethane; water; acetone; at -25 - 20 ℃; for 1.5h;
DOI:10.1016/j.tet.2010.11.017

Reference yield: 88.0%

: C₁₅H₂₀O₃

: 1195988-16-9
C₁₅H₂₀O₄

Guidance literature:: With titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; Cumene hydroperoxide; In dichloromethane; at -40 - -25 ℃; for 9h; Molecular sieve;
DOI:10.1021/ol902217q

Reference yield:

: 1195988-14-7
C₂₃H₃₆O₄Si

: 1195988-16-9
C₁₅H₂₀O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 - -50 °C

1.2: -78 - 20 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 13 h / 0 - 20 °C

3.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; Cumene hydroperoxide / dichloromethane / 9 h / -40 - -25 °C / Molecular sieve

3.2: 1.5 h / -25 - 20 °C

With titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; Cumene hydroperoxide; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; In tetrahydrofuran; hexane; dichloromethane; 3.1: Sharpless epoxidation;
DOI:10.1016/j.tet.2010.11.017