(R)-1-[2-(3-benzyloxypropyl)-6-propyl-1,4,5,6-tetrahydropyridin-3-yl]-propan-1-one

Base Information

Chemical Name:(R)-1-[2-(3-benzyloxypropyl)-6-propyl-1,4,5,6-tetrahydropyridin-3-yl]-propan-1-one
CAS No.:865433-85-8
Molecular Formula:C₂₁H₃₁NO₂
Molecular Weight:329.483
Hs Code.:

Synonyms:(R)-1-[2-(3-benzyloxypropyl)-6-propyl-1,4,5,6-tetrahydropyridin-3-yl]-propan-1-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-1-[2-(3-benzyloxypropyl)-6-propyl-1,4,5,6-tetrahydropyridin-3-yl]-propan-1-one

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Technology Process of (R)-1-[2-(3-benzyloxypropyl)-6-propyl-1,4,5,6-tetrahydropyridin-3-yl]-propan-1-one

There total 4 articles about (R)-1-[2-(3-benzyloxypropyl)-6-propyl-1,4,5,6-tetrahydropyridin-3-yl]-propan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 8-benzoxy-4-decyn-3-one

: (R)-1-chloro-3-hexylamine hydrochloride salt

: 865433-85-8
(R)-1-[2-(3-benzyloxypropyl)-6-propyl-1,4,5,6-tetrahydropyridin-3-yl]-propan-1-one

Guidance literature:: With sodium carbonate; sodium iodide; In isopropyl alcohol; for 30h; Heating;
DOI:10.1021/jo051080y

Reference yield:

: Benzyl-[(R)-1-(2-chloro-ethyl)-butyl]-((R)-1-phenyl-ethyl)-amine

: 865433-85-8
(R)-1-[2-(3-benzyloxypropyl)-6-propyl-1,4,5,6-tetrahydropyridin-3-yl]-propan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd(OH)2/C / methanol / 48 h / 30 °C / 38000 Torr

2: 66 percent / Na₂CO₃; NaI / propan-2-ol / 30 h / Heating

With hydrogen; sodium carbonate; sodium iodide; palladium dihydroxide; In methanol; isopropyl alcohol;
DOI:10.1021/jo051080y

Reference yield:

: (3R)-3-{benzyl[(1R)-1-phenylethyl]amino}hexan-1-ol

: 865433-85-8
(R)-1-[2-(3-benzyloxypropyl)-6-propyl-1,4,5,6-tetrahydropyridin-3-yl]-propan-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / CHCl₃ / 1 h / Heating

2: H₂ / Pd(OH)2/C / methanol / 48 h / 30 °C / 38000 Torr

3: 66 percent / Na₂CO₃; NaI / propan-2-ol / 30 h / Heating

With thionyl chloride; hydrogen; sodium carbonate; sodium iodide; palladium dihydroxide; In methanol; chloroform; isopropyl alcohol;
DOI:10.1021/jo051080y