2-methoxymethoxy-5-n-hexadecylbenzaldehyde

Base Information

Chemical Name:2-methoxymethoxy-5-n-hexadecylbenzaldehyde
CAS No.:611227-42-0
Molecular Formula:C₂₅H₄₂O₃
Molecular Weight:390.607
Hs Code.:

Synonyms:2-methoxymethoxy-5-n-hexadecylbenzaldehyde

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Chemical Property of 2-methoxymethoxy-5-n-hexadecylbenzaldehyde

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Technology Process of 2-methoxymethoxy-5-n-hexadecylbenzaldehyde

There total 5 articles about 2-methoxymethoxy-5-n-hexadecylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 611227-34-0
1-hexadecyl-4-methoxymethoxy-benzene

: 611227-42-0
2-methoxymethoxy-5-n-hexadecylbenzaldehyde

Guidance literature:: 1-hexadecyl-4-methoxymethoxy-benzene; With n-butyllithium; In tetrahydrofuran; hexane; at -5 ℃; for 0.5h;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; toluene; at -5 ℃; for 1h;

Reference yield:

: 2589-78-8
4-hexadecylphenol

: 611227-42-0
2-methoxymethoxy-5-n-hexadecylbenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: 99.7 percent / methyltrioctylammonium chloride; NaOH / CH₂Cl₂; H₂O / 0.5 h / -10 °C

2.1: butyllithium / tetrahydrofuran; hexane / 0.5 h / -5 °C

2.2: 99 percent / tetrahydrofuran; hexane; toluene / 1 h / -5 °C

With sodium hydroxide; n-butyllithium; Aliquat 336; In tetrahydrofuran; hexane; dichloromethane; water;

Reference yield:

: 2589-76-6
1-(4-hydroxyphenyl)hexadecane-1-one

: 611227-42-0
2-methoxymethoxy-5-n-hexadecylbenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: 43 percent / zinc powder; HgCl₂; HCl / ethanol; H₂O / Heating

2.1: 99.7 percent / methyltrioctylammonium chloride; NaOH / CH₂Cl₂; H₂O / 0.5 h / -10 °C

3.1: butyllithium / tetrahydrofuran; hexane / 0.5 h / -5 °C

3.2: 99 percent / tetrahydrofuran; hexane; toluene / 1 h / -5 °C

With hydrogenchloride; sodium hydroxide; n-butyllithium; Aliquat 336; mercury dichloride; zinc; In tetrahydrofuran; ethanol; hexane; dichloromethane; water;